Chemical Mediated Synthesis of Polyaniline/Tungstenoxide (PANI/WO3) Nanocomposites and Their Antibacterial Activity Against Clinical Pathogenic Bacteria
Polyaniline and tungsten oxide (PANI/WO 3 )-doped nanocomposites were synthesised by in situ chemical oxidation technique using different weight percentage of WO 3 (10%, 30% and 50%), and the polymerization of PANI was carried out by using ammonium persulphate as an oxidising agent. These nanocompos...
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Veröffentlicht in: | BioNanoScience 2020-03, Vol.10 (1), p.73-80 |
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Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | Polyaniline and tungsten oxide (PANI/WO
3
)-doped nanocomposites were synthesised by in situ chemical oxidation technique using different weight percentage of WO
3
(10%, 30% and 50%), and the polymerization of PANI was carried out by using ammonium persulphate as an oxidising agent. These nanocomposites are characterized by physical methods, viz., Fourier transform infrared spectra (FTIR), X-ray diffraction (XRD) and scanning electron microscope (SEM). The X-ray pattern confirmed that the formation of polyaniline and SEM micrographs exhibited agglomeration and showed that WO
3
particles have a strong effect on the morphology of composites with average grain sizes of 10–20 nm. FTIR spectra revealed the strong bonding between PANI and WO
3
particles. Further, these nanocomposites doped with 10% (P1), 30% (P3) and 50% (P5) of WO
3
were tested for their antibacterial activity against pathogenic bacteria, viz.,
Escherichia coli
,
Enterobacter aerogenes
,
Pseudomonas aeruginosa
and
Salmonella typhimurium
. Results revealed that these nanocomposites had shown potential antibacterial activity against all the tested pathogenic strains which was confirmed by clear zone of inhibition. |
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ISSN: | 2191-1630 2191-1649 |
DOI: | 10.1007/s12668-019-00679-z |