Hexagonal diameter in cadmium sulfide/anodic alumina nanoporous bi-layer membrane by a sol–gel spin coating and their sensing application
Cadmium sulfide/anodic alumina nanoporous bi-layer film was designed for the first time by two-step anodization followed by a sol–gel spin coating method. The chemical composition, morphological, electrical and structural properties of the AA and Cd/AA nanoporous membranes have been examined. The mo...
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Veröffentlicht in: | Applied physics. A, Materials science & processing Materials science & processing, 2020-04, Vol.126 (4), Article 268 |
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Sprache: | eng |
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Zusammenfassung: | Cadmium sulfide/anodic alumina nanoporous bi-layer film was designed for the first time by two-step anodization followed by a sol–gel spin coating method. The chemical composition, morphological, electrical and structural properties of the AA and Cd/AA nanoporous membranes have been examined. The morphological investigation of AA layer demonstrates the development of an exceptionally ordered hexagonal exhibit of nanoporous anodic alumina of pore diameter ~ 55 nm and inter-pore distance ~ 125 nm. Though, CdS/AA demonstrated the deposition of nanoporous CdS layer from agglomerated CdS nanoparticles on the surface of the membrane of AA. The energy-dispersive X-ray spectrum of CdS/AA outlined signs of O, Al, Cd, and S, which shows its high purity. The X-ray diffraction affirmed the development of cubic-phase CdS in the favored (220) orientation with normal ~ 86.2 nm crystallite size. The present voltage and resistance–concentration attributes of the CdS/AA layer as a glucose biosensor are fitted well with second-order polynomial behavior (correlation coefficient = 0.981). The glucose concentration changed from 0 to 400 mg/dl. In light of the upsides of the fabrication approach, this new age of minimal effort biosensors can be utilized as a guarantee building block for nanophotonic and nanoelectronic gadgets. |
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ISSN: | 0947-8396 1432-0630 |
DOI: | 10.1007/s00339-020-3371-5 |