Viscous flow assisted sintering of AlCoCrFeNi high entropy alloy powder
[Display omitted] •This work studies the sintering mechanisms of AlCoCrFeNi HEA powder.•Activation energy of 166 ± 13 kJ/mol, was found to be in the range of reported literature data of similar alloys.•Formed viscous phase at higher temperature was found to be Cr-rich phase. Present investigation at...
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Veröffentlicht in: | Materials letters 2019-12, Vol.256, p.126668, Article 126668 |
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Format: | Artikel |
Sprache: | eng |
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•This work studies the sintering mechanisms of AlCoCrFeNi HEA powder.•Activation energy of 166 ± 13 kJ/mol, was found to be in the range of reported literature data of similar alloys.•Formed viscous phase at higher temperature was found to be Cr-rich phase.
Present investigation attempts to evaluate the sintering kinetics of mechanically alloyed AlCoCrFeNi high entropy alloy powder. Dilatometric study shows an accelerated densification above 1150 °C during non-isothermal sintering. The process was characterized with an activation energy of 166 ± 13 kJ/mol. Sintering was found to be controlled by the viscous flow mechanisms and atomic diffusion of constituent elements in the melt phase. This was attributed to the formation of some Cr-rich viscous phase, which had a good wettability on the solid. Results were further confirmed by an endothermic peak during differential scanning calorimetry and the solidified phases around the grains, in the quenched microstructure. |
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ISSN: | 0167-577X 1873-4979 |
DOI: | 10.1016/j.matlet.2019.126668 |