Hot compressive deformation behavior and electron backscattering diffraction analysis of Mg95.50Zn3.71Y0.79 fine-grained alloy solidified under high pressure

An Mg 95.50 Zn 3.71 Y 0.79 fine-grained solidified alloy with a grain size of 16 μm was prepared by high-pressure solidification. The microstructure characteristics and hot compressive deformation behavior of the alloy solidified under high pressure were compared with the atmospheric-pressure solidi...

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Veröffentlicht in:Journal of materials science 2018-02, Vol.53 (4), p.2880-2891
Hauptverfasser: Zhibin, Fan, Xiaoping, Lin, Yun, Dong, Rui, Xu, Lin, Wang
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Yun, Dong
Rui, Xu
Lin, Wang
description An Mg 95.50 Zn 3.71 Y 0.79 fine-grained solidified alloy with a grain size of 16 μm was prepared by high-pressure solidification. The microstructure characteristics and hot compressive deformation behavior of the alloy solidified under high pressure were compared with the atmospheric-pressure solidified alloy by carrying out the unilateral compression tests under a strain rate in the range of 0.001–1.0 s −1 and at a deformation temperature in the range of 523–573 K. The true stress-true strain curve of the high-pressure solidified alloy shows the typical dynamic recrystallization rheological curve. EBSD results show that when the deformation was carried out at 573 K, nearly 90% dynamic recrystallization occurred in the high-pressure solidified alloy, and the newly formed grains were distortionless and had low dislocation density. The high-pressure solidified alloy showed a double-peak basal texture at a strain rate of 1.0 s −1 . The two peak points showed a maximum pole density of 9.88 and 7.91, less than that in atmospheric-pressure alloy. When the deformation was carried out at the following conditions: deformation temperature = 573 K, strain rate = 0.001, and true strain = 0.9, the average Schmid factor (SF) for basal slip of the grains in the high-pressure solidified alloy was 0.419, and SF value for basal slip in 91% grains was greater than 0.3.
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The microstructure characteristics and hot compressive deformation behavior of the alloy solidified under high pressure were compared with the atmospheric-pressure solidified alloy by carrying out the unilateral compression tests under a strain rate in the range of 0.001–1.0 s −1 and at a deformation temperature in the range of 523–573 K. The true stress-true strain curve of the high-pressure solidified alloy shows the typical dynamic recrystallization rheological curve. EBSD results show that when the deformation was carried out at 573 K, nearly 90% dynamic recrystallization occurred in the high-pressure solidified alloy, and the newly formed grains were distortionless and had low dislocation density. The high-pressure solidified alloy showed a double-peak basal texture at a strain rate of 1.0 s −1 . The two peak points showed a maximum pole density of 9.88 and 7.91, less than that in atmospheric-pressure alloy. 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The microstructure characteristics and hot compressive deformation behavior of the alloy solidified under high pressure were compared with the atmospheric-pressure solidified alloy by carrying out the unilateral compression tests under a strain rate in the range of 0.001–1.0 s −1 and at a deformation temperature in the range of 523–573 K. The true stress-true strain curve of the high-pressure solidified alloy shows the typical dynamic recrystallization rheological curve. EBSD results show that when the deformation was carried out at 573 K, nearly 90% dynamic recrystallization occurred in the high-pressure solidified alloy, and the newly formed grains were distortionless and had low dislocation density. The high-pressure solidified alloy showed a double-peak basal texture at a strain rate of 1.0 s −1 . The two peak points showed a maximum pole density of 9.88 and 7.91, less than that in atmospheric-pressure alloy. When the deformation was carried out at the following conditions: deformation temperature = 573 K, strain rate = 0.001, and true strain = 0.9, the average Schmid factor (SF) for basal slip of the grains in the high-pressure solidified alloy was 0.419, and SF value for basal slip in 91% grains was greater than 0.3.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10853-017-1698-x</doi><tpages>12</tpages></addata></record>
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subjects Characterization and Evaluation of Materials
Chemistry and Materials Science
Classical Mechanics
Compression tests
Crystallography and Scattering Methods
Deformation
Dislocation density
Dynamic recrystallization
Electron backscatter diffraction
Grain size
Materials Science
Metals
Polymer Sciences
Rheological properties
Slip
Solid Mechanics
Solidification
Strain rate
True strain
True stress
title Hot compressive deformation behavior and electron backscattering diffraction analysis of Mg95.50Zn3.71Y0.79 fine-grained alloy solidified under high pressure
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