Preparation of Titanate/N-Doped Anatase Composite Hierarchical Microspheres with Enhanced Visible Light Photocatalytic Activity

Titanate/N-doped anatase composite hierarchical microspheres have been obtained by calcination treatment of NH 4 -titanate hierarchical microspheres at proper temperatures. The phase structure is dependent on the calcination temperature and varies from titanate to anatase with increasing calcination...

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Veröffentlicht in:Catalysis letters 2015-02, Vol.145 (2), p.647-653
Hauptverfasser: Qiu, Yong, Wu, Liangpeng, Li, Juan, Li, Xinjun
Format: Artikel
Sprache:eng
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Zusammenfassung:Titanate/N-doped anatase composite hierarchical microspheres have been obtained by calcination treatment of NH 4 -titanate hierarchical microspheres at proper temperatures. The phase structure is dependent on the calcination temperature and varies from titanate to anatase with increasing calcination temperature, with the heterophase in-between. The composite structure is verified by the results of XRD, visible and UV Raman spectra. The titanate/N-doped anatase composite sample calcined at 300 °C for 1 h exhibits enhanced activity in the degradation of Rhodamine B under visible light irradiation compared to the other samples. The enhanced activity can be ascribed to the synergistic effect of titanate and N-doped anatase. Graphical Abstract
ISSN:1011-372X
1572-879X
DOI:10.1007/s10562-014-1423-1