Elastic constants of β-Ti15Mo

Elastic constants of single crystals of metastable β-titanium Ti15Mo alloy (in wt. %), grown in an optical floating zone furnace, were measured by resonant ultrasound spectroscopy with the aim to study the dependence of these constants on formation of isothermal ω particles. Samples with different h...

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Veröffentlicht in:Journal of alloys and compounds 2019-07, Vol.792, p.960-967
Hauptverfasser: Nejezchlebová, Jitka, Janovská, Michaela, Sedlák, Petr, Šmilauerová, Jana, Stráský, Josef, Janeček, Miloš, Seiner, Hanuš
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Sprache:eng
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Zusammenfassung:Elastic constants of single crystals of metastable β-titanium Ti15Mo alloy (in wt. %), grown in an optical floating zone furnace, were measured by resonant ultrasound spectroscopy with the aim to study the dependence of these constants on formation of isothermal ω particles. Samples with different heat treatment (isothermal/anisothermal ageing at different temperatures) were studied. Ultrasonic measurements were complemented by characterization of the samples by transmission electron microscopy. The results proved that isothermal ω particles always exactly follow the original cubic symmetry of the β matrix and that the evolution of the elastic constants of the β-ω multi-phase crystals and the volume fraction of ω phase can be reliably approximated using Hill's homogenizing procedure, assuming cubic elastic constants of the β phase and isotropic elastic constants representing ω particles. It was shown that ultrasonic methods can be used for the study of the evolution of microstructure of metastable β-titanium alloys due to the high contrast in elastic moduli of the β and ω phases. •Single crystals of β-Ti15Mo were studied by resonant ultrasound spectroscopy.•Resonant ultrasound spectroscopy is highly sensitive to change of ω volume fraction.•Growth of ω phase causes the stiffening and isotropisation of the material.•Volume fraction of ω phase was approximated via Hill's homogenization.
ISSN:0925-8388
1873-4669
DOI:10.1016/j.jallcom.2019.03.418