Determination of the Active Hydrogen Content in a Pyridine-Borane Complex by Schiff Base Reduction and High-Performance Liquid Chromatography

A study describes a simple, rapid and reproducible method for quantitating the active hydrogen content in pyridine-borane complex. The method exploits the ease with which Schiff bases are reduced by amine-boranes and uses high-performance liquid chromatography to quantitate the reduction product.

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Bibliographische Detailangaben
Veröffentlicht in:	Analytical chemistry (Washington) 1994-12, Vol.66 (23), p.4283-4287
Hauptverfasser:	Morley, James A, Elrod, Lee, Bauer, John F
Format:	Artikel
Sprache:	eng
Schlagworte:	Analytical chemistry Chemistry Chromatographic methods and physical methods associated with chromatography Exact sciences and technology Hydrogen Organic chemistry Other chromatographic methods
Online-Zugang:	Volltext
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Beschreibung
Zusammenfassung:	A study describes a simple, rapid and reproducible method for quantitating the active hydrogen content in pyridine-borane complex. The method exploits the ease with which Schiff bases are reduced by amine-boranes and uses high-performance liquid chromatography to quantitate the reduction product.
ISSN:	0003-2700 1520-6882
DOI:	10.1021/ac00095a026