Convenient Synthesis of a Lactone, γ-Butyrolactone
A five-membered cyclic ester, gamma-Butyrolactone, was prepared from GHB using a microscale reflux method. Cyclization yielded a product with a boiling point significantly greater (by 129 °C) than that of the open-chain analogue.
Gespeichert in:
Veröffentlicht in: | Journal of chemical education 1998-01, Vol.75 (1), p.84 |
---|---|
Hauptverfasser: | , , |
Format: | Artikel |
Sprache: | eng |
Schlagworte: | |
Online-Zugang: | Volltext |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
container_end_page | |
---|---|
container_issue | 1 |
container_start_page | 84 |
container_title | Journal of chemical education |
container_volume | 75 |
creator | Bozak, Richard E Knittel, J Hicks, Ronald J |
description | A five-membered cyclic ester, gamma-Butyrolactone, was prepared from GHB using a microscale reflux method. Cyclization yielded a product with a boiling point significantly greater (by 129 °C) than that of the open-chain analogue. |
doi_str_mv | 10.1021/ed075p84 |
format | Article |
fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_211914138</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>25175463</sourcerecordid><originalsourceid>FETCH-LOGICAL-a281t-b273209427f7743a734131a5c4e6ef24fc5c852f844d8c36ebef59778471b89b3</originalsourceid><addsrcrecordid>eNplkM1KxDAUhYMoWEfBRyjiwoXV3PxMkqUW_6DgQl2XNJNgh7GpSSr0ueY9fCYrVVy4OnDPx3fhIHQM-AIwgUu7woL3ku2gDBSVBVAid1GGp65QXLJ9dBDjGmMgXMkM0dJ3H7ZrbZfyp7FLrza2Mfcu13mlTfKdPc8_t8X1kMbgN_PlEO05vYn26CcX6OX25rm8L6rHu4fyqio0kZCKhghKsGJEOCEY1YIyoKC5YXZpHWHOcCM5cZKxlTR0aRvruBJCMgGNVA1doJPZ2wf_PtiY6rUfQje9rAmAgkknJ-hshkzwMQbr6j60bzqMNeD6e5H6d5EJPZ1RbeKf6h_2BUpSXZo</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>211914138</pqid></control><display><type>article</type><title>Convenient Synthesis of a Lactone, γ-Butyrolactone</title><source>American Chemical Society Journals</source><creator>Bozak, Richard E ; Knittel, J ; Hicks, Ronald J</creator><creatorcontrib>Bozak, Richard E ; Knittel, J ; Hicks, Ronald J</creatorcontrib><description>A five-membered cyclic ester, gamma-Butyrolactone, was prepared from GHB using a microscale reflux method. Cyclization yielded a product with a boiling point significantly greater (by 129 °C) than that of the open-chain analogue.</description><identifier>ISSN: 0021-9584</identifier><identifier>EISSN: 1938-1328</identifier><identifier>DOI: 10.1021/ed075p84</identifier><identifier>CODEN: JCEDA8</identifier><language>eng</language><publisher>Easton: Division of Chemical Education</publisher><subject>Butyrolactone ; Experiments ; Organic chemistry ; Science education</subject><ispartof>Journal of chemical education, 1998-01, Vol.75 (1), p.84</ispartof><rights>Copyright American Chemical Society Jan 1998</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-a281t-b273209427f7743a734131a5c4e6ef24fc5c852f844d8c36ebef59778471b89b3</citedby></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://pubs.acs.org/doi/pdf/10.1021/ed075p84$$EPDF$$P50$$Gacs$$H</linktopdf><linktohtml>$$Uhttps://pubs.acs.org/doi/10.1021/ed075p84$$EHTML$$P50$$Gacs$$H</linktohtml><link.rule.ids>314,780,784,2764,27075,27923,27924,56737,56787</link.rule.ids></links><search><creatorcontrib>Bozak, Richard E</creatorcontrib><creatorcontrib>Knittel, J</creatorcontrib><creatorcontrib>Hicks, Ronald J</creatorcontrib><title>Convenient Synthesis of a Lactone, γ-Butyrolactone</title><title>Journal of chemical education</title><addtitle>J. Chem. Educ</addtitle><description>A five-membered cyclic ester, gamma-Butyrolactone, was prepared from GHB using a microscale reflux method. Cyclization yielded a product with a boiling point significantly greater (by 129 °C) than that of the open-chain analogue.</description><subject>Butyrolactone</subject><subject>Experiments</subject><subject>Organic chemistry</subject><subject>Science education</subject><issn>0021-9584</issn><issn>1938-1328</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1998</creationdate><recordtype>article</recordtype><sourceid>8G5</sourceid><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AIMQZ</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><sourceid>GUQSH</sourceid><sourceid>M2O</sourceid><recordid>eNplkM1KxDAUhYMoWEfBRyjiwoXV3PxMkqUW_6DgQl2XNJNgh7GpSSr0ueY9fCYrVVy4OnDPx3fhIHQM-AIwgUu7woL3ku2gDBSVBVAid1GGp65QXLJ9dBDjGmMgXMkM0dJ3H7ZrbZfyp7FLrza2Mfcu13mlTfKdPc8_t8X1kMbgN_PlEO05vYn26CcX6OX25rm8L6rHu4fyqio0kZCKhghKsGJEOCEY1YIyoKC5YXZpHWHOcCM5cZKxlTR0aRvruBJCMgGNVA1doJPZ2wf_PtiY6rUfQje9rAmAgkknJ-hshkzwMQbr6j60bzqMNeD6e5H6d5EJPZ1RbeKf6h_2BUpSXZo</recordid><startdate>199801</startdate><enddate>199801</enddate><creator>Bozak, Richard E</creator><creator>Knittel, J</creator><creator>Hicks, Ronald J</creator><general>Division of Chemical Education</general><general>American Chemical Society</general><scope>AAYXX</scope><scope>CITATION</scope><scope>0-V</scope><scope>3V.</scope><scope>7X7</scope><scope>7XB</scope><scope>88B</scope><scope>88E</scope><scope>88I</scope><scope>8A4</scope><scope>8FE</scope><scope>8FG</scope><scope>8FI</scope><scope>8FJ</scope><scope>8FK</scope><scope>8G5</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AEUYN</scope><scope>AFKRA</scope><scope>AIMQZ</scope><scope>ALSLI</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>BHPHI</scope><scope>BKSAR</scope><scope>CCPQU</scope><scope>CJNVE</scope><scope>D1I</scope><scope>DWQXO</scope><scope>FYUFA</scope><scope>GHDGH</scope><scope>GNUQQ</scope><scope>GUQSH</scope><scope>HCIFZ</scope><scope>K9.</scope><scope>KB.</scope><scope>LIQON</scope><scope>M0P</scope><scope>M0S</scope><scope>M1P</scope><scope>M2O</scope><scope>M2P</scope><scope>MBDVC</scope><scope>PADUT</scope><scope>PCBAR</scope><scope>PDBOC</scope><scope>PQEDU</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>Q9U</scope></search><sort><creationdate>199801</creationdate><title>Convenient Synthesis of a Lactone, γ-Butyrolactone</title><author>Bozak, Richard E ; Knittel, J ; Hicks, Ronald J</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-a281t-b273209427f7743a734131a5c4e6ef24fc5c852f844d8c36ebef59778471b89b3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1998</creationdate><topic>Butyrolactone</topic><topic>Experiments</topic><topic>Organic chemistry</topic><topic>Science education</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Bozak, Richard E</creatorcontrib><creatorcontrib>Knittel, J</creatorcontrib><creatorcontrib>Hicks, Ronald J</creatorcontrib><collection>CrossRef</collection><collection>ProQuest Social Sciences Premium Collection</collection><collection>ProQuest Central (Corporate)</collection><collection>Health & Medical Collection</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>Education Database (Alumni Edition)</collection><collection>Medical Database (Alumni Edition)</collection><collection>Science Database (Alumni Edition)</collection><collection>Education Periodicals</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Hospital Premium Collection</collection><collection>Hospital Premium Collection (Alumni Edition)</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>Research Library (Alumni Edition)</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest One Sustainability</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest One Literature</collection><collection>Social Science Premium Collection</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>Natural Science Collection (ProQuest)</collection><collection>Earth, Atmospheric & Aquatic Science Collection</collection><collection>ProQuest One Community College</collection><collection>Education Collection</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>Health Research Premium Collection</collection><collection>Health Research Premium Collection (Alumni)</collection><collection>ProQuest Central Student</collection><collection>Research Library Prep</collection><collection>SciTech Premium Collection</collection><collection>ProQuest Health & Medical Complete (Alumni)</collection><collection>Materials Science Database</collection><collection>ProQuest One Literature - U.S. Customers Only</collection><collection>Education Database</collection><collection>Health & Medical Collection (Alumni Edition)</collection><collection>Medical Database</collection><collection>Research Library</collection><collection>Science Database (ProQuest)</collection><collection>Research Library (Corporate)</collection><collection>Research Library China</collection><collection>Earth, Atmospheric & Aquatic Science Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Education</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>ProQuest Central Basic</collection><jtitle>Journal of chemical education</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Bozak, Richard E</au><au>Knittel, J</au><au>Hicks, Ronald J</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Convenient Synthesis of a Lactone, γ-Butyrolactone</atitle><jtitle>Journal of chemical education</jtitle><addtitle>J. Chem. Educ</addtitle><date>1998-01</date><risdate>1998</risdate><volume>75</volume><issue>1</issue><spage>84</spage><pages>84-</pages><issn>0021-9584</issn><eissn>1938-1328</eissn><coden>JCEDA8</coden><abstract>A five-membered cyclic ester, gamma-Butyrolactone, was prepared from GHB using a microscale reflux method. Cyclization yielded a product with a boiling point significantly greater (by 129 °C) than that of the open-chain analogue.</abstract><cop>Easton</cop><pub>Division of Chemical Education</pub><doi>10.1021/ed075p84</doi></addata></record> |
fulltext | fulltext |
identifier | ISSN: 0021-9584 |
ispartof | Journal of chemical education, 1998-01, Vol.75 (1), p.84 |
issn | 0021-9584 1938-1328 |
language | eng |
recordid | cdi_proquest_journals_211914138 |
source | American Chemical Society Journals |
subjects | Butyrolactone Experiments Organic chemistry Science education |
title | Convenient Synthesis of a Lactone, γ-Butyrolactone |
url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-09T10%3A05%3A32IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Convenient%20Synthesis%20of%20a%20Lactone,%20%CE%B3-Butyrolactone&rft.jtitle=Journal%20of%20chemical%20education&rft.au=Bozak,%20Richard%20E&rft.date=1998-01&rft.volume=75&rft.issue=1&rft.spage=84&rft.pages=84-&rft.issn=0021-9584&rft.eissn=1938-1328&rft.coden=JCEDA8&rft_id=info:doi/10.1021/ed075p84&rft_dat=%3Cproquest_cross%3E25175463%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=211914138&rft_id=info:pmid/&rfr_iscdi=true |