Solution Combustion Synthesis of BiFeO3 Powders Using CTAB as Fuel
Nearly pure BiFeO 3 powders were synthesized by the solution combustion method using cetyltrimethylammonium bromide as fuel at various fuel to oxidant ratios ( φ ). Phase evolution, morphology, magnetic and optical properties were characterized by thermal analysis, infrared spectroscopy, x-ray diffr...
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creator | Asefi, N. Hasheminiasari, M. Masoudpanah, S. M. |
description | Nearly pure BiFeO
3
powders were synthesized by the solution combustion method using cetyltrimethylammonium bromide as fuel at various fuel to oxidant ratios (
φ
). Phase evolution, morphology, magnetic and optical properties were characterized by thermal analysis, infrared spectroscopy, x-ray diffractometry, electron microscopy, photoluminescence and diffuse reflectance spectroscopy techniques, respectively. An impurity Bi
24
Fe
2
O
39
phase appeared while increasing the fuel content. Magnetization of the as-combusted BiFeO
3
powders increased from 0.5 emu/g to 11.1 emu/g on account of the decrease in particle size and appearance of the impurity phase with the increase of
φ
values. Visible light absorption and band gap energy depended on the purity and morphology, being tunable by fuel content. About 85% of methylene blue was photodegraded in the presence of the powders prepared by
φ
= 0.5 under visible light irradiation. |
doi_str_mv | 10.1007/s11664-018-6722-7 |
format | Article |
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3
powders were synthesized by the solution combustion method using cetyltrimethylammonium bromide as fuel at various fuel to oxidant ratios (
φ
). Phase evolution, morphology, magnetic and optical properties were characterized by thermal analysis, infrared spectroscopy, x-ray diffractometry, electron microscopy, photoluminescence and diffuse reflectance spectroscopy techniques, respectively. An impurity Bi
24
Fe
2
O
39
phase appeared while increasing the fuel content. Magnetization of the as-combusted BiFeO
3
powders increased from 0.5 emu/g to 11.1 emu/g on account of the decrease in particle size and appearance of the impurity phase with the increase of
φ
values. Visible light absorption and band gap energy depended on the purity and morphology, being tunable by fuel content. About 85% of methylene blue was photodegraded in the presence of the powders prepared by
φ
= 0.5 under visible light irradiation.</description><identifier>ISSN: 0361-5235</identifier><identifier>EISSN: 1543-186X</identifier><identifier>DOI: 10.1007/s11664-018-6722-7</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Bismuth ferrite ; Cetyltrimethylammonium bromide ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Combustion synthesis ; Diffuse reflectance spectroscopy ; Electromagnetic absorption ; Electronics and Microelectronics ; Energy gap ; Fuels ; Impurities ; Infrared analysis ; Instrumentation ; Light irradiation ; Magnetic properties ; Materials Science ; Methylene blue ; Morphology ; Optical and Electronic Materials ; Optical properties ; Photoluminescence ; Solid State Physics ; Spectrum analysis ; Thermal analysis</subject><ispartof>Journal of electronic materials, 2019-01, Vol.48 (1), p.409-415</ispartof><rights>The Minerals, Metals & Materials Society 2018</rights><rights>Journal of Electronic Materials is a copyright of Springer, (2018). All Rights Reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c353t-2a75aded74d97714eba7296187fd56de95c6f3e12b2bb189308fc539e3a020733</citedby><cites>FETCH-LOGICAL-c353t-2a75aded74d97714eba7296187fd56de95c6f3e12b2bb189308fc539e3a020733</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11664-018-6722-7$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11664-018-6722-7$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Asefi, N.</creatorcontrib><creatorcontrib>Hasheminiasari, M.</creatorcontrib><creatorcontrib>Masoudpanah, S. M.</creatorcontrib><title>Solution Combustion Synthesis of BiFeO3 Powders Using CTAB as Fuel</title><title>Journal of electronic materials</title><addtitle>Journal of Elec Materi</addtitle><description>Nearly pure BiFeO
3
powders were synthesized by the solution combustion method using cetyltrimethylammonium bromide as fuel at various fuel to oxidant ratios (
φ
). Phase evolution, morphology, magnetic and optical properties were characterized by thermal analysis, infrared spectroscopy, x-ray diffractometry, electron microscopy, photoluminescence and diffuse reflectance spectroscopy techniques, respectively. An impurity Bi
24
Fe
2
O
39
phase appeared while increasing the fuel content. Magnetization of the as-combusted BiFeO
3
powders increased from 0.5 emu/g to 11.1 emu/g on account of the decrease in particle size and appearance of the impurity phase with the increase of
φ
values. Visible light absorption and band gap energy depended on the purity and morphology, being tunable by fuel content. About 85% of methylene blue was photodegraded in the presence of the powders prepared by
φ
= 0.5 under visible light irradiation.</description><subject>Bismuth ferrite</subject><subject>Cetyltrimethylammonium bromide</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Combustion synthesis</subject><subject>Diffuse reflectance spectroscopy</subject><subject>Electromagnetic absorption</subject><subject>Electronics and Microelectronics</subject><subject>Energy gap</subject><subject>Fuels</subject><subject>Impurities</subject><subject>Infrared analysis</subject><subject>Instrumentation</subject><subject>Light irradiation</subject><subject>Magnetic properties</subject><subject>Materials Science</subject><subject>Methylene blue</subject><subject>Morphology</subject><subject>Optical and Electronic Materials</subject><subject>Optical properties</subject><subject>Photoluminescence</subject><subject>Solid State Physics</subject><subject>Spectrum analysis</subject><subject>Thermal analysis</subject><issn>0361-5235</issn><issn>1543-186X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><sourceid>8G5</sourceid><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><sourceid>GUQSH</sourceid><sourceid>M2O</sourceid><recordid>eNp1kE1LAzEQhoMoWKs_wFvAczSTbJLdY7vYKhQqtAVvYT-ydUu7qZldpP_erSt48jRzeJ93mIeQe-CPwLl5QgCtI8YhZtoIwcwFGYGKJINYv1-SEZcamBJSXZMbxB3noCCGEZmu_L5ra9_Q1B_yDn_W1alpPxzWSH1Fp_XMLSV981-lC0g3WDdbmq4nU5ohnXVuf0uuqmyP7u53jslm9rxOX9hiOX9NJwtWSCVbJjKjstKVJioTYyByeWZEoiE2Val06RJV6Eo6ELnIc4gTyeOqUDJxMuOCGynH5GHoPQb_2Tls7c53oelPWgH9m0IrrvoUDKkieMTgKnsM9SELJwvcnlXZQZXtVdmzKmt6RgwM9tlm68Jf8__QN4Dzacs</recordid><startdate>20190101</startdate><enddate>20190101</enddate><creator>Asefi, N.</creator><creator>Hasheminiasari, M.</creator><creator>Masoudpanah, S. M.</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>7XB</scope><scope>88I</scope><scope>8AF</scope><scope>8AO</scope><scope>8FE</scope><scope>8FG</scope><scope>8FK</scope><scope>8G5</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>ARAPS</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>GNUQQ</scope><scope>GUQSH</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>L6V</scope><scope>M2O</scope><scope>M2P</scope><scope>M7S</scope><scope>MBDVC</scope><scope>P5Z</scope><scope>P62</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope><scope>Q9U</scope><scope>S0X</scope></search><sort><creationdate>20190101</creationdate><title>Solution Combustion Synthesis of BiFeO3 Powders Using CTAB as Fuel</title><author>Asefi, N. ; Hasheminiasari, M. ; Masoudpanah, S. M.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c353t-2a75aded74d97714eba7296187fd56de95c6f3e12b2bb189308fc539e3a020733</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2019</creationdate><topic>Bismuth ferrite</topic><topic>Cetyltrimethylammonium bromide</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Combustion synthesis</topic><topic>Diffuse reflectance spectroscopy</topic><topic>Electromagnetic absorption</topic><topic>Electronics and Microelectronics</topic><topic>Energy gap</topic><topic>Fuels</topic><topic>Impurities</topic><topic>Infrared analysis</topic><topic>Instrumentation</topic><topic>Light irradiation</topic><topic>Magnetic properties</topic><topic>Materials Science</topic><topic>Methylene blue</topic><topic>Morphology</topic><topic>Optical and Electronic Materials</topic><topic>Optical properties</topic><topic>Photoluminescence</topic><topic>Solid State Physics</topic><topic>Spectrum analysis</topic><topic>Thermal analysis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Asefi, N.</creatorcontrib><creatorcontrib>Hasheminiasari, M.</creatorcontrib><creatorcontrib>Masoudpanah, S. 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M.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Solution Combustion Synthesis of BiFeO3 Powders Using CTAB as Fuel</atitle><jtitle>Journal of electronic materials</jtitle><stitle>Journal of Elec Materi</stitle><date>2019-01-01</date><risdate>2019</risdate><volume>48</volume><issue>1</issue><spage>409</spage><epage>415</epage><pages>409-415</pages><issn>0361-5235</issn><eissn>1543-186X</eissn><abstract>Nearly pure BiFeO
3
powders were synthesized by the solution combustion method using cetyltrimethylammonium bromide as fuel at various fuel to oxidant ratios (
φ
). Phase evolution, morphology, magnetic and optical properties were characterized by thermal analysis, infrared spectroscopy, x-ray diffractometry, electron microscopy, photoluminescence and diffuse reflectance spectroscopy techniques, respectively. An impurity Bi
24
Fe
2
O
39
phase appeared while increasing the fuel content. Magnetization of the as-combusted BiFeO
3
powders increased from 0.5 emu/g to 11.1 emu/g on account of the decrease in particle size and appearance of the impurity phase with the increase of
φ
values. Visible light absorption and band gap energy depended on the purity and morphology, being tunable by fuel content. About 85% of methylene blue was photodegraded in the presence of the powders prepared by
φ
= 0.5 under visible light irradiation.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s11664-018-6722-7</doi><tpages>7</tpages></addata></record> |
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subjects | Bismuth ferrite Cetyltrimethylammonium bromide Characterization and Evaluation of Materials Chemistry and Materials Science Combustion synthesis Diffuse reflectance spectroscopy Electromagnetic absorption Electronics and Microelectronics Energy gap Fuels Impurities Infrared analysis Instrumentation Light irradiation Magnetic properties Materials Science Methylene blue Morphology Optical and Electronic Materials Optical properties Photoluminescence Solid State Physics Spectrum analysis Thermal analysis |
title | Solution Combustion Synthesis of BiFeO3 Powders Using CTAB as Fuel |
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