Solution Combustion Synthesis of BiFeO3 Powders Using CTAB as Fuel

Nearly pure BiFeO 3 powders were synthesized by the solution combustion method using cetyltrimethylammonium bromide as fuel at various fuel to oxidant ratios ( φ ). Phase evolution, morphology, magnetic and optical properties were characterized by thermal analysis, infrared spectroscopy, x-ray diffr...

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Veröffentlicht in:Journal of electronic materials 2019-01, Vol.48 (1), p.409-415
Hauptverfasser: Asefi, N., Hasheminiasari, M., Masoudpanah, S. M.
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Masoudpanah, S. M.
description Nearly pure BiFeO 3 powders were synthesized by the solution combustion method using cetyltrimethylammonium bromide as fuel at various fuel to oxidant ratios ( φ ). Phase evolution, morphology, magnetic and optical properties were characterized by thermal analysis, infrared spectroscopy, x-ray diffractometry, electron microscopy, photoluminescence and diffuse reflectance spectroscopy techniques, respectively. An impurity Bi 24 Fe 2 O 39 phase appeared while increasing the fuel content. Magnetization of the as-combusted BiFeO 3 powders increased from 0.5 emu/g to 11.1 emu/g on account of the decrease in particle size and appearance of the impurity phase with the increase of φ values. Visible light absorption and band gap energy depended on the purity and morphology, being tunable by fuel content. About 85% of methylene blue was photodegraded in the presence of the powders prepared by φ  = 0.5 under visible light irradiation.
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subjects Bismuth ferrite
Cetyltrimethylammonium bromide
Characterization and Evaluation of Materials
Chemistry and Materials Science
Combustion synthesis
Diffuse reflectance spectroscopy
Electromagnetic absorption
Electronics and Microelectronics
Energy gap
Fuels
Impurities
Infrared analysis
Instrumentation
Light irradiation
Magnetic properties
Materials Science
Methylene blue
Morphology
Optical and Electronic Materials
Optical properties
Photoluminescence
Solid State Physics
Spectrum analysis
Thermal analysis
title Solution Combustion Synthesis of BiFeO3 Powders Using CTAB as Fuel
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