Morphology and Structure of a Fine-Grained Composite Material Based on Boehmite Extracted from Aqueous Solutions of Na-Carboxymethyl Cellulose with Aluminum Powder
Fine-grained composite material is synthesized from aluminum powder in aqueous solutions of Na-sodium carboxymethyl cellulose. The phase composition of the composite material is determined using X-ray phase analysis and infrared spectroscopy. Aluminum oxyhydroxide (boehmite) stabilized by the polyme...
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Veröffentlicht in: | Surface investigation, x-ray, synchrotron and neutron techniques x-ray, synchrotron and neutron techniques, 2018-09, Vol.12 (5), p.974-981 |
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Hauptverfasser: | , , |
Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | Fine-grained composite material is synthesized from aluminum powder in aqueous solutions of Na-sodium carboxymethyl cellulose. The phase composition of the composite material is determined using X-ray phase analysis and infrared spectroscopy. Aluminum oxyhydroxide (boehmite) stabilized by the polymer material Na-sodium carboxymethyl cellulose is found to be formed during synthesis. The interaction between boehmite and the polymer material is implemented due to intermolecular hydrogen bonds. The formation of 600-nm spherical particles with porous surfaces is revealed by scanning electron microscopy. Unlike traditional methods of producing boehmite at 200–400°С, synthesis occurs at 70–80°С. The prospects of using boehmite for the creation of porous functional materials are shown. |
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ISSN: | 1027-4510 1819-7094 |
DOI: | 10.1134/S102745101805021X |