Facile hydrothermal synthesis of cobalt stannate (Co2SnO4) nano particles for electrochemical properties
In recent decades, super capacitor is considered to be a prime candidate for the next generation of electrochemical applications. In the present work, nano structured pure Co 2 SnO 4 nanoparticles (Co 2 SnO 4 NPs) were successfully synthesized by a facile hydrothermal method using sodium hydroxide a...
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Veröffentlicht in: | Journal of materials science. Materials in electronics 2017-03, Vol.28 (6), p.4780-4787 |
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Hauptverfasser: | , , , |
Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | In recent decades, super capacitor is considered to be a prime candidate for the next generation of electrochemical applications. In the present work, nano structured pure Co
2
SnO
4
nanoparticles (Co
2
SnO
4
NPs) were successfully synthesized by a facile hydrothermal method using sodium hydroxide as a mineralizer. This synthesized product calcinated at 900 °C was used to the formation of cubic structured Co
2
SnO
4
NPs, which is confirmed through TG/DT analysis. Crystalline phase and the mean crystalline size of the Co
2
SnO
4
NPs were evaluated from the XRD study. Surface morphology of Co
2
SnO
4
NPs was confirmed by FE-SEM and HRTEM analysis. Hydrodynamic size distribution and surface potential were measured by using dynamic light scattering. From the FT-IR study, the presences of Co–O and Sn–O vibrations were identified. Cyclic voltammetry measurement, the specific capacitance value was calculated as 596 F g
−1
at a scan rate 2 mV s
−1
for Co
2
SnO
4
NPs which paves way for the super capacitor applications. |
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ISSN: | 0957-4522 1573-482X |
DOI: | 10.1007/s10854-016-6123-8 |