Synthesis and Characterization of Amino-Terminated Chloration Modified Peanut Shell and Its Application to Preconcentrate and Detect the Concentration of Sunset Yellow in Drink and Jelly Samples
Sunset yellow, as a common pigment, is harmful to people’s health. In this work, a new sensitive adsorbent based on the chlorination peanut shell and HBP-NH 2 was fabricated via one-step synthesis. Optimization of the modified peanut shell was carried out at different temperatures, different molar r...
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Veröffentlicht in: | Food analytical methods 2018-08, Vol.11 (8), p.2158-2171 |
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creator | Lin, Baohong Li, Song Fang, Lei Zhu, Minliang Xiong, Chunhua |
description | Sunset yellow, as a common pigment, is harmful to people’s health. In this work, a new sensitive adsorbent based on the chlorination peanut shell and HBP-NH
2
was fabricated via one-step synthesis. Optimization of the modified peanut shell was carried out at different temperatures, different molar ratios of reagents, and different time intervals in HBP-NH
2
using Response Surface Methodology (RSM) for the first attempt. The structure of modified peanut shell was characterized by FT-IR, SEM, and TGA analysis. The adsorption properties of the modified peanut shell for Sunset yellow were investigated by batch and column experiments. Batch adsorption’s results suggested that modified peanut shell had a high adsorption capability for Sunset yellow and its maximum saturated adsorption capacity was 468.0 mg/g at 308 K, estimated from the Langmuir model. Furthermore, the modified peanut shell can be eluted easily using 3 mol/L NaOH. The proposed method was successfully applied to quantify the amount of SY in jelly and soft drinks with good recovery valuing from 98 to 104%. Hence, the proposed sensor shows a rapid and sensitive method, low cost, and simple, which is appropriate for alternative technique use for the analysis of food colorants in commercial products. |
doi_str_mv | 10.1007/s12161-018-1175-4 |
format | Article |
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2
was fabricated via one-step synthesis. Optimization of the modified peanut shell was carried out at different temperatures, different molar ratios of reagents, and different time intervals in HBP-NH
2
using Response Surface Methodology (RSM) for the first attempt. The structure of modified peanut shell was characterized by FT-IR, SEM, and TGA analysis. The adsorption properties of the modified peanut shell for Sunset yellow were investigated by batch and column experiments. Batch adsorption’s results suggested that modified peanut shell had a high adsorption capability for Sunset yellow and its maximum saturated adsorption capacity was 468.0 mg/g at 308 K, estimated from the Langmuir model. Furthermore, the modified peanut shell can be eluted easily using 3 mol/L NaOH. The proposed method was successfully applied to quantify the amount of SY in jelly and soft drinks with good recovery valuing from 98 to 104%. Hence, the proposed sensor shows a rapid and sensitive method, low cost, and simple, which is appropriate for alternative technique use for the analysis of food colorants in commercial products.</description><identifier>ISSN: 1936-9751</identifier><identifier>EISSN: 1936-976X</identifier><identifier>DOI: 10.1007/s12161-018-1175-4</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Adsorption ; Analytical Chemistry ; Beverages ; Chemistry ; Chemistry and Materials Science ; Chemistry/Food Science ; Columns (structural) ; Food analysis ; Food dyes ; Food production ; Food Science ; Infrared radiation ; Microbiology ; Optimization ; Peanuts ; Reagents ; Response surface methodology ; Sodium hydroxide ; Soft drinks ; Sunset ; Synthesis</subject><ispartof>Food analytical methods, 2018-08, Vol.11 (8), p.2158-2171</ispartof><rights>Springer Science+Business Media, LLC, part of Springer Nature 2018</rights><rights>Copyright Springer Science & Business Media 2018</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c316t-f86452616618b1f49cc518110c718d007ef97f24dde0bf974994215e2c11c9633</citedby><cites>FETCH-LOGICAL-c316t-f86452616618b1f49cc518110c718d007ef97f24dde0bf974994215e2c11c9633</cites><orcidid>0000-0001-8695-1912</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s12161-018-1175-4$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s12161-018-1175-4$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27903,27904,41467,42536,51297</link.rule.ids></links><search><creatorcontrib>Lin, Baohong</creatorcontrib><creatorcontrib>Li, Song</creatorcontrib><creatorcontrib>Fang, Lei</creatorcontrib><creatorcontrib>Zhu, Minliang</creatorcontrib><creatorcontrib>Xiong, Chunhua</creatorcontrib><title>Synthesis and Characterization of Amino-Terminated Chloration Modified Peanut Shell and Its Application to Preconcentrate and Detect the Concentration of Sunset Yellow in Drink and Jelly Samples</title><title>Food analytical methods</title><addtitle>Food Anal. Methods</addtitle><description>Sunset yellow, as a common pigment, is harmful to people’s health. In this work, a new sensitive adsorbent based on the chlorination peanut shell and HBP-NH
2
was fabricated via one-step synthesis. Optimization of the modified peanut shell was carried out at different temperatures, different molar ratios of reagents, and different time intervals in HBP-NH
2
using Response Surface Methodology (RSM) for the first attempt. The structure of modified peanut shell was characterized by FT-IR, SEM, and TGA analysis. The adsorption properties of the modified peanut shell for Sunset yellow were investigated by batch and column experiments. Batch adsorption’s results suggested that modified peanut shell had a high adsorption capability for Sunset yellow and its maximum saturated adsorption capacity was 468.0 mg/g at 308 K, estimated from the Langmuir model. Furthermore, the modified peanut shell can be eluted easily using 3 mol/L NaOH. The proposed method was successfully applied to quantify the amount of SY in jelly and soft drinks with good recovery valuing from 98 to 104%. Hence, the proposed sensor shows a rapid and sensitive method, low cost, and simple, which is appropriate for alternative technique use for the analysis of food colorants in commercial products.</description><subject>Adsorption</subject><subject>Analytical Chemistry</subject><subject>Beverages</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chemistry/Food Science</subject><subject>Columns (structural)</subject><subject>Food analysis</subject><subject>Food dyes</subject><subject>Food production</subject><subject>Food Science</subject><subject>Infrared radiation</subject><subject>Microbiology</subject><subject>Optimization</subject><subject>Peanuts</subject><subject>Reagents</subject><subject>Response surface methodology</subject><subject>Sodium hydroxide</subject><subject>Soft drinks</subject><subject>Sunset</subject><subject>Synthesis</subject><issn>1936-9751</issn><issn>1936-976X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><recordid>eNp1kctOwzAQRSMEEs8PYGeJdcDjJk6yrMqrCARSiwQry3Um1JDawXaFyufxZbgNghWrGc3ce8byTZJjoKdAaXHmgQGHlEKZAhR5mm0le1ANeFoV_Gn7t89hN9n3_pVSTjNge8nXZGXCHL32RJqajObSSRXQ6U8ZtDXENmS40MamU3SxyoBrUWtdv76ztW50nD2gNMtAJnNs2w1pHDwZdl2rVa8Mljw4VNYoNCG6caM6x4AqkPgCMvpd_dydLI3HQJ4j0X4Qbci50-ZtY7uJsxWZyEXXoj9MdhrZejz6qQfJ4-XFdHSd3t5fjUfD21QNgIe0KXmWMw6cQzmDJquUyqEEoKqAso5_iE1VNCyra6Sz2GZVlTHIkSkAVfHB4CA56bmds-9L9EG82qUz8aRgNEILFvlRBb1KOeu9w0Z0Ti-kWwmgYh2V6KMSMSqxjkpk0cN6j49a84Luj_y_6RtizZle</recordid><startdate>20180801</startdate><enddate>20180801</enddate><creator>Lin, Baohong</creator><creator>Li, Song</creator><creator>Fang, Lei</creator><creator>Zhu, Minliang</creator><creator>Xiong, Chunhua</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><orcidid>https://orcid.org/0000-0001-8695-1912</orcidid></search><sort><creationdate>20180801</creationdate><title>Synthesis and Characterization of Amino-Terminated Chloration Modified Peanut Shell and Its Application to Preconcentrate and Detect the Concentration of Sunset Yellow in Drink and Jelly Samples</title><author>Lin, Baohong ; Li, Song ; Fang, Lei ; Zhu, Minliang ; Xiong, Chunhua</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c316t-f86452616618b1f49cc518110c718d007ef97f24dde0bf974994215e2c11c9633</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Adsorption</topic><topic>Analytical Chemistry</topic><topic>Beverages</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Chemistry/Food Science</topic><topic>Columns (structural)</topic><topic>Food analysis</topic><topic>Food dyes</topic><topic>Food production</topic><topic>Food Science</topic><topic>Infrared radiation</topic><topic>Microbiology</topic><topic>Optimization</topic><topic>Peanuts</topic><topic>Reagents</topic><topic>Response surface methodology</topic><topic>Sodium hydroxide</topic><topic>Soft drinks</topic><topic>Sunset</topic><topic>Synthesis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Lin, Baohong</creatorcontrib><creatorcontrib>Li, Song</creatorcontrib><creatorcontrib>Fang, Lei</creatorcontrib><creatorcontrib>Zhu, Minliang</creatorcontrib><creatorcontrib>Xiong, Chunhua</creatorcontrib><collection>CrossRef</collection><jtitle>Food analytical methods</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Lin, Baohong</au><au>Li, Song</au><au>Fang, Lei</au><au>Zhu, Minliang</au><au>Xiong, Chunhua</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and Characterization of Amino-Terminated Chloration Modified Peanut Shell and Its Application to Preconcentrate and Detect the Concentration of Sunset Yellow in Drink and Jelly Samples</atitle><jtitle>Food analytical methods</jtitle><stitle>Food Anal. Methods</stitle><date>2018-08-01</date><risdate>2018</risdate><volume>11</volume><issue>8</issue><spage>2158</spage><epage>2171</epage><pages>2158-2171</pages><issn>1936-9751</issn><eissn>1936-976X</eissn><abstract>Sunset yellow, as a common pigment, is harmful to people’s health. In this work, a new sensitive adsorbent based on the chlorination peanut shell and HBP-NH
2
was fabricated via one-step synthesis. Optimization of the modified peanut shell was carried out at different temperatures, different molar ratios of reagents, and different time intervals in HBP-NH
2
using Response Surface Methodology (RSM) for the first attempt. The structure of modified peanut shell was characterized by FT-IR, SEM, and TGA analysis. The adsorption properties of the modified peanut shell for Sunset yellow were investigated by batch and column experiments. Batch adsorption’s results suggested that modified peanut shell had a high adsorption capability for Sunset yellow and its maximum saturated adsorption capacity was 468.0 mg/g at 308 K, estimated from the Langmuir model. Furthermore, the modified peanut shell can be eluted easily using 3 mol/L NaOH. The proposed method was successfully applied to quantify the amount of SY in jelly and soft drinks with good recovery valuing from 98 to 104%. Hence, the proposed sensor shows a rapid and sensitive method, low cost, and simple, which is appropriate for alternative technique use for the analysis of food colorants in commercial products.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s12161-018-1175-4</doi><tpages>14</tpages><orcidid>https://orcid.org/0000-0001-8695-1912</orcidid></addata></record> |
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source | Springer Nature - Complete Springer Journals |
subjects | Adsorption Analytical Chemistry Beverages Chemistry Chemistry and Materials Science Chemistry/Food Science Columns (structural) Food analysis Food dyes Food production Food Science Infrared radiation Microbiology Optimization Peanuts Reagents Response surface methodology Sodium hydroxide Soft drinks Sunset Synthesis |
title | Synthesis and Characterization of Amino-Terminated Chloration Modified Peanut Shell and Its Application to Preconcentrate and Detect the Concentration of Sunset Yellow in Drink and Jelly Samples |
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