Synthesis and Characterization of Amino-Terminated Chloration Modified Peanut Shell and Its Application to Preconcentrate and Detect the Concentration of Sunset Yellow in Drink and Jelly Samples

Sunset yellow, as a common pigment, is harmful to people’s health. In this work, a new sensitive adsorbent based on the chlorination peanut shell and HBP-NH 2 was fabricated via one-step synthesis. Optimization of the modified peanut shell was carried out at different temperatures, different molar r...

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Veröffentlicht in:Food analytical methods 2018-08, Vol.11 (8), p.2158-2171
Hauptverfasser: Lin, Baohong, Li, Song, Fang, Lei, Zhu, Minliang, Xiong, Chunhua
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container_title Food analytical methods
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creator Lin, Baohong
Li, Song
Fang, Lei
Zhu, Minliang
Xiong, Chunhua
description Sunset yellow, as a common pigment, is harmful to people’s health. In this work, a new sensitive adsorbent based on the chlorination peanut shell and HBP-NH 2 was fabricated via one-step synthesis. Optimization of the modified peanut shell was carried out at different temperatures, different molar ratios of reagents, and different time intervals in HBP-NH 2 using Response Surface Methodology (RSM) for the first attempt. The structure of modified peanut shell was characterized by FT-IR, SEM, and TGA analysis. The adsorption properties of the modified peanut shell for Sunset yellow were investigated by batch and column experiments. Batch adsorption’s results suggested that modified peanut shell had a high adsorption capability for Sunset yellow and its maximum saturated adsorption capacity was 468.0 mg/g at 308 K, estimated from the Langmuir model. Furthermore, the modified peanut shell can be eluted easily using 3 mol/L NaOH. The proposed method was successfully applied to quantify the amount of SY in jelly and soft drinks with good recovery valuing from 98 to 104%. Hence, the proposed sensor shows a rapid and sensitive method, low cost, and simple, which is appropriate for alternative technique use for the analysis of food colorants in commercial products.
doi_str_mv 10.1007/s12161-018-1175-4
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The proposed method was successfully applied to quantify the amount of SY in jelly and soft drinks with good recovery valuing from 98 to 104%. 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subjects Adsorption
Analytical Chemistry
Beverages
Chemistry
Chemistry and Materials Science
Chemistry/Food Science
Columns (structural)
Food analysis
Food dyes
Food production
Food Science
Infrared radiation
Microbiology
Optimization
Peanuts
Reagents
Response surface methodology
Sodium hydroxide
Soft drinks
Sunset
Synthesis
title Synthesis and Characterization of Amino-Terminated Chloration Modified Peanut Shell and Its Application to Preconcentrate and Detect the Concentration of Sunset Yellow in Drink and Jelly Samples
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