Synthesis and Characterization of Amino-Terminated Chloration Modified Peanut Shell and Its Application to Preconcentrate and Detect the Concentration of Sunset Yellow in Drink and Jelly Samples
Sunset yellow, as a common pigment, is harmful to people’s health. In this work, a new sensitive adsorbent based on the chlorination peanut shell and HBP-NH 2 was fabricated via one-step synthesis. Optimization of the modified peanut shell was carried out at different temperatures, different molar r...
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Veröffentlicht in: | Food analytical methods 2018-08, Vol.11 (8), p.2158-2171 |
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Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | Sunset yellow, as a common pigment, is harmful to people’s health. In this work, a new sensitive adsorbent based on the chlorination peanut shell and HBP-NH
2
was fabricated via one-step synthesis. Optimization of the modified peanut shell was carried out at different temperatures, different molar ratios of reagents, and different time intervals in HBP-NH
2
using Response Surface Methodology (RSM) for the first attempt. The structure of modified peanut shell was characterized by FT-IR, SEM, and TGA analysis. The adsorption properties of the modified peanut shell for Sunset yellow were investigated by batch and column experiments. Batch adsorption’s results suggested that modified peanut shell had a high adsorption capability for Sunset yellow and its maximum saturated adsorption capacity was 468.0 mg/g at 308 K, estimated from the Langmuir model. Furthermore, the modified peanut shell can be eluted easily using 3 mol/L NaOH. The proposed method was successfully applied to quantify the amount of SY in jelly and soft drinks with good recovery valuing from 98 to 104%. Hence, the proposed sensor shows a rapid and sensitive method, low cost, and simple, which is appropriate for alternative technique use for the analysis of food colorants in commercial products. |
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ISSN: | 1936-9751 1936-976X |
DOI: | 10.1007/s12161-018-1175-4 |