Molecular and Crystal Structure of the Condensation Product of 2-(7-Bromo-2-Oxo-5-Phenyl-3H-1,4-Benzdiazepin-1-Yl)Acetohydrazide (Gidazepam) with Salicylic Aldehyde

Molecular and Crystal Structure of the Condensation Product of 2-(7-Bromo-2-Oxo-5-Phenyl-3H-1,4-Benzdiazepin-1-Yl)Acetohydrazide (Gidazepam) with Salicylic Aldehyde

Hydrazone [HydrHSal]∙Н 2 О is synthesized for the first time by the interaction of 2-(7-bromo-2-oxo-5- phenyl-3 H -1,4-benzdiazepin-1-yl)acetohydrazide (gidazepam) with salicylic aldehyde and characterized by the elemental analysis, thermogravimetry, mass, electron, IR, and NMR spectroscopic techniq...

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Veröffentlicht in:Journal of structural chemistry 2018-03, Vol.59 (2), p.497-501
Hauptverfasser: Pulya, A. V., Seifullina, I. I., Skorokhod, L. S., Pavlovskii, V. I., Kravtsov, V. Kh, Bogza, S. L., Suikov, S. Yu
Format: Artikel
Sprache:eng
Schlagworte:
Atomic
Atomic/Molecular Structure and Spectra
Chemistry
Chemistry and Materials Science
Condensates
Crystal structure
Diffraction
Hydrazones
Infrared radiation
Inorganic Chemistry
Molecular
Molecular chains
Molecular structure
NMR
Nuclear magnetic resonance
Optical and Plasma Physics
Physical Chemistry
Single crystals
Solid State Physics
Thermogravimetry
X-ray diffraction
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Zusammenfassung:Hydrazone [HydrHSal]∙Н 2 О is synthesized for the first time by the interaction of 2-(7-bromo-2-oxo-5- phenyl-3 H -1,4-benzdiazepin-1-yl)acetohydrazide (gidazepam) with salicylic aldehyde and characterized by the elemental analysis, thermogravimetry, mass, electron, IR, and NMR spectroscopic techniques. The molecular and crystal structure is determined by single crystal X-ray diffraction.
ISSN:0022-4766
1573-8779
DOI:10.1134/S002247661802035X