One-Pot Synthesis of Phenylhydrazones from Alkenes

One-Pot Synthesis of Phenylhydrazones from Alkenes

A one-pot procedure has been developed for the synthesis of phenylhydrazones by ozonolysis of olefins in methanol at 0°C and subsequent reduction of peroxide intermediate with excess 1: 2 mixture of phenylhydrazine hydrochloride and sodium acetate.

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Bibliographische Detailangaben
Veröffentlicht in:Russian journal of organic chemistry 2018, Vol.54 (1), p.51-54
Hauptverfasser: Legostaeva, Yu. V., Garifullina, L. R., Nazarov, I. S., Ishmuratov, G. Yu
Format: Artikel
Sprache:eng
Schlagworte:
Alkenes
Chemistry
Chemistry and Materials Science
Organic Chemistry
Sodium acetate
Synthesis
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Beschreibung
Zusammenfassung:A one-pot procedure has been developed for the synthesis of phenylhydrazones by ozonolysis of olefins in methanol at 0°C and subsequent reduction of peroxide intermediate with excess 1: 2 mixture of phenylhydrazine hydrochloride and sodium acetate.
ISSN:1070-4280
1608-3393
DOI:10.1134/S1070428018010037