Solvothermal Decomposition of α-Co(OH)2@SDS in n-Octanol

Solvothermal Decomposition of α-Co(OH)2@SDS in n-Octanol

The solvothermal decomposition of a hybrid organic–inorganic material based on α-Со(ОН) 2 and sodium dodecyl sulfate has been studied in n-octanol at 190°C and the atmospheric pressure. It has been found that the process includes two stages: in the first stage, anhydrous CoCO 3 is formed, followed b...

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Veröffentlicht in:Russian journal of inorganic chemistry 2018-02, Vol.63 (2), p.245-250
Hauptverfasser: Pikurova, E. V., Saikova, S. V., Pashkov, G. L., Panteleeva, M. V., Mikhlin, Yu. L.
Format: Artikel
Sprache:eng
Schlagworte:
Chemistry
Chemistry and Materials Science
Cobalt oxides
Decomposition
Inorganic Chemistry
Octanol
Physical Methods of Investigation
Sodium dodecyl sulfate
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Zusammenfassung:The solvothermal decomposition of a hybrid organic–inorganic material based on α-Со(ОН) 2 and sodium dodecyl sulfate has been studied in n-octanol at 190°C and the atmospheric pressure. It has been found that the process includes two stages: in the first stage, anhydrous CoCO 3 is formed, followed by its topochemical decomposition to form Co 3 O 4 . It has been found that products consist of rhombic-shaped particles about 250 nm in size.
ISSN:0036-0236
1531-8613
DOI:10.1134/S0036023618020171