Synthesis of 2,3-Dihydro[1,4]oxazino[2,3,4-ij]quinolinium Bromide and Its Reaction with Sodium Hydroxide

The reaction of quinolin-8-ol with 1,2-dibromoethane in dimethylformamide gave 2,3-dihydro[1,4]-oxazino[2,3,4- ij ]quinolinium bromide which reacted with aqueous sodium hydroxide to afford 2,3,4,5-tetrahydro[1,4]oxazino[2,3,4- ij ]quinoline, 2,3,4,5-tetrahydro[1,4]oxazino[2,3,4- ij ]quinolin-5-ol, a...

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Veröffentlicht in:Russian journal of general chemistry 2018, Vol.88 (1), p.127-130
Hauptverfasser: Kim, D. G., Vasilenko, A. V., Melent’ev, A. B.
Format: Artikel
Sprache:eng
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Zusammenfassung:The reaction of quinolin-8-ol with 1,2-dibromoethane in dimethylformamide gave 2,3-dihydro[1,4]-oxazino[2,3,4- ij ]quinolinium bromide which reacted with aqueous sodium hydroxide to afford 2,3,4,5-tetrahydro[1,4]oxazino[2,3,4- ij ]quinoline, 2,3,4,5-tetrahydro[1,4]oxazino[2,3,4- ij ]quinolin-5-ol, and 2,3,4,5-tetrahydro[1,4]oxazino[2,3,4- ij ]quinolin-5-one.
ISSN:1070-3632
1608-3350
DOI:10.1134/S1070363218010218