Particle anisotropy and crystalline phase transition in one-pot synthesis of nano-zirconia: a causal relationship

Crystalline phase evolution and morphological changes are strictly correlated phenomena during the growth of zirconia nanoparticles. In this work, the effects of synthetic variables, reaction time (up to 24 hours) and precursor concentration (0.16 and 0.5 M), of a one-step non-hydrolytic sol–gel rou...

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Veröffentlicht in:	CrystEngComm 2018, Vol.20 (7), p.879-888
Hauptverfasser:	Tana, Francesca, Serafini, Andrea, Lutterotti, Luca, Cigada, Alberto, Variola, Fabio, Bondioli, Federica, De Nardo, Luigi
Format:	Artikel
Sprache:	eng
Schlagworte:	Benzyl alcohol Crystal structure Crystallinity Diffraction patterns Electron diffraction Electrons Microstructure Particle size distribution Phase transitions Reaction time Sol-gel processes Transmission electron microscopy X-ray diffraction Zirconium dioxide Zirconium oxides
Online-Zugang:	Volltext
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