Ultra-Performance Liquid Chromatography-Triple Quadruple Mass Spectrometry (UPLC-TQ/MS) for Evaluation of Biogenic Amines in Wine

In this study, a fast, simple, and sensitive analytical method for direct determination of biogenic amines tryptamine, putrescine, histamine, phenylethylamine, tyramine, cadaverine, spermine, and spermidine in wine has been developed and validated. Detection of analytes was performed with ultra-perf...

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Veröffentlicht in:	Food analytical methods 2017-12, Vol.10 (12), p.4038-4048
Hauptverfasser:	Tašev, Krste, Ivanova-Petropulos, Violeta, Stefova, Marina
Format:	Artikel
Sprache:	eng
Schlagworte:	Amines Analytical Chemistry Biogenic amines Cadaverine Chemistry Chemistry and Materials Science Chemistry/Food Science Chromatography Correlation coefficients Food Science Histamine Liquid chromatography Mass spectrometry Mass spectroscopy Microbiology Phenethylamine Phenylethylamine Putrescine Reproducibility Spermidine Spermine Tryptamine Tyramine Wines
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Zusammenfassung:	In this study, a fast, simple, and sensitive analytical method for direct determination of biogenic amines tryptamine, putrescine, histamine, phenylethylamine, tyramine, cadaverine, spermine, and spermidine in wine has been developed and validated. Detection of analytes was performed with ultra-performance liquid chromatography (UPLC) coupled to triple quadruple mass spectrometer (TQ/MS). The calibration curves of all amines were linear with correlation coefficients ( R 2 ) ranging from 0.9906 for putrescine to 0.9998 for histamine and 2-phenyethylamine. The accuracy of the method was checked with a standard addition method, showing good accuracy, repeatability, and reproducibility ( RSD
ISSN:	1936-9751 1936-976X
DOI:	10.1007/s12161-017-0936-9