Synthesis of polymer nanogels by electro-Fenton process: investigation of the effect of main operation parameters

Synthesis of polymer nanogels by electro-Fenton process: investigation of the effect of main operation parameters

[Display omitted] •Synthesis of PVP nanogels by electro-Fenton: a facile, low cost, environmentally-friendly route.•In situ production of OH and HO2 based on H2O2 electrogeneration and Fe2+ addition.•Semi-dilute PVP, 0.5–1.0mmoldm−3 Fe2+, low j and short t: Rh

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Veröffentlicht in:Electrochimica acta 2017-08, Vol.246, p.812-822
Hauptverfasser: Lanzalaco, Sonia, Sirés, Ignasi, Sabatino, Maria Antonietta, Dispenza, Clelia, Scialdone, Onofrio, Galia, Alessandro
Format: Artikel
Sprache:eng
Schlagworte:
Biocompatibility
Biomedical materials
Chain mobility
Chain scission
Chemical synthesis
Cleavage
Conjugation
Crosslinking
Electro-Fenton process
Electrocatalysis
Electrochemical synthesis
Electrolysis
Gas-diffusion electrode
Hydroxyl radical
Liquid chromatography
Low cost
Molecular weight
Polymer crosslinking
Polymers
Process parameters
Size reduction
Studies
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Zusammenfassung:[Display omitted] •Synthesis of PVP nanogels by electro-Fenton: a facile, low cost, environmentally-friendly route.•In situ production of OH and HO2 based on H2O2 electrogeneration and Fe2+ addition.•Semi-dilute PVP, 0.5–1.0mmoldm−3 Fe2+, low j and short t: Rh
ISSN:0013-4686
1873-3859
DOI:10.1016/j.electacta.2017.06.097