Evaluation of mesoporous imprinted silicas as MSPD selective sorbents of ketoprofen in powder milk
•New mesoporous imprinted silicas were prepared using ketoprofen as template.•Materials were evaluated as sorbent in matrix solid phase dispersion for extraction of NSAIDs.•Results show that SBA-15-MIS-2 is appropriate to selective extraction of ketoprofen in powder milk. Two molecularly imprinted m...
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| Veröffentlicht in: | Materials letters 2017-06, Vol.197, p.5-7 |
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| container_title | Materials letters |
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| creator | Gañán, J. Morante-Zarcero, S. Pérez-Quintanilla, D. Sierra, I. |
| description | •New mesoporous imprinted silicas were prepared using ketoprofen as template.•Materials were evaluated as sorbent in matrix solid phase dispersion for extraction of NSAIDs.•Results show that SBA-15-MIS-2 is appropriate to selective extraction of ketoprofen in powder milk.
Two molecularly imprinted mesoporous silicas were synthesized using different ratios of ketoprofen as template molecule and amino-functionalized SBA-15 as support. The materials synthesized were characterized and evaluated as selective sorbents for matrix solid phase dispersion (MSPD) of ketoprofen in the presence of other nonsteroidal anti-inflammatory drugs (NSAIDs) in powder milk samples. |
| doi_str_mv | 10.1016/j.matlet.2017.03.137 |
| format | Article |
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Two molecularly imprinted mesoporous silicas were synthesized using different ratios of ketoprofen as template molecule and amino-functionalized SBA-15 as support. The materials synthesized were characterized and evaluated as selective sorbents for matrix solid phase dispersion (MSPD) of ketoprofen in the presence of other nonsteroidal anti-inflammatory drugs (NSAIDs) in powder milk samples.</description><identifier>ISSN: 0167-577X</identifier><identifier>EISSN: 1873-4979</identifier><identifier>DOI: 10.1016/j.matlet.2017.03.137</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Chemical synthesis ; Imprinted mesoporous silica ; Ketoprofen ; Materials science ; Milk ; Molecular imprinting ; MSPD ; Nonsteroidal anti-inflammatory drugs ; NSAIDs ; Silica ; Sorbents</subject><ispartof>Materials letters, 2017-06, Vol.197, p.5-7</ispartof><rights>2017 Elsevier B.V.</rights><rights>Copyright Elsevier BV Jun 15, 2017</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c334t-edb136fb81f08cf00bdb37d62b6015e234de2c82648c0bfa78d7bd7a2f5684813</citedby><cites>FETCH-LOGICAL-c334t-edb136fb81f08cf00bdb37d62b6015e234de2c82648c0bfa78d7bd7a2f5684813</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.matlet.2017.03.137$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3548,27922,27923,45993</link.rule.ids></links><search><creatorcontrib>Gañán, J.</creatorcontrib><creatorcontrib>Morante-Zarcero, S.</creatorcontrib><creatorcontrib>Pérez-Quintanilla, D.</creatorcontrib><creatorcontrib>Sierra, I.</creatorcontrib><title>Evaluation of mesoporous imprinted silicas as MSPD selective sorbents of ketoprofen in powder milk</title><title>Materials letters</title><description>•New mesoporous imprinted silicas were prepared using ketoprofen as template.•Materials were evaluated as sorbent in matrix solid phase dispersion for extraction of NSAIDs.•Results show that SBA-15-MIS-2 is appropriate to selective extraction of ketoprofen in powder milk.
Two molecularly imprinted mesoporous silicas were synthesized using different ratios of ketoprofen as template molecule and amino-functionalized SBA-15 as support. The materials synthesized were characterized and evaluated as selective sorbents for matrix solid phase dispersion (MSPD) of ketoprofen in the presence of other nonsteroidal anti-inflammatory drugs (NSAIDs) in powder milk samples.</description><subject>Chemical synthesis</subject><subject>Imprinted mesoporous silica</subject><subject>Ketoprofen</subject><subject>Materials science</subject><subject>Milk</subject><subject>Molecular imprinting</subject><subject>MSPD</subject><subject>Nonsteroidal anti-inflammatory drugs</subject><subject>NSAIDs</subject><subject>Silica</subject><subject>Sorbents</subject><issn>0167-577X</issn><issn>1873-4979</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><recordid>eNp9kE9LAzEQxYMoWKvfwEPA867JJt1sL4LU-gcqCip4C5tkAml3N2uSVvz2ptSzMDCX997M-yF0SUlJCa2v12Xfpg5SWREqSsJKysQRmtBGsILPxfwYTbJMFDMhPk_RWYxrQgifEz5Barlru22bnB-wt7iH6Ecf_DZi14_BDQkMjq5zuo04z_Pb6x2O0IFObgc4-qBgSHFv3UDyY_AWBuwGPPpvAwH3rtucoxPbdhEu_vYUfdwv3xePxerl4Wlxuyo0YzwVYBRltVUNtaTRlhBlFBOmrlRN6Awqxg1Uuqlq3miibCsaI5QRbWVndcMbyqbo6pCbv_jaQkxy7bdhyCclnXNWU1GJOqv4QaWDjzGAlblm34YfSYnc05RreaAp9zQlYTLTzLabgw1yg52DIKN2MGgwLmQY0nj3f8Avh1CBcg</recordid><startdate>20170615</startdate><enddate>20170615</enddate><creator>Gañán, J.</creator><creator>Morante-Zarcero, S.</creator><creator>Pérez-Quintanilla, D.</creator><creator>Sierra, I.</creator><general>Elsevier B.V</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20170615</creationdate><title>Evaluation of mesoporous imprinted silicas as MSPD selective sorbents of ketoprofen in powder milk</title><author>Gañán, J. ; Morante-Zarcero, S. ; Pérez-Quintanilla, D. ; Sierra, I.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c334t-edb136fb81f08cf00bdb37d62b6015e234de2c82648c0bfa78d7bd7a2f5684813</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Chemical synthesis</topic><topic>Imprinted mesoporous silica</topic><topic>Ketoprofen</topic><topic>Materials science</topic><topic>Milk</topic><topic>Molecular imprinting</topic><topic>MSPD</topic><topic>Nonsteroidal anti-inflammatory drugs</topic><topic>NSAIDs</topic><topic>Silica</topic><topic>Sorbents</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Gañán, J.</creatorcontrib><creatorcontrib>Morante-Zarcero, S.</creatorcontrib><creatorcontrib>Pérez-Quintanilla, D.</creatorcontrib><creatorcontrib>Sierra, I.</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Materials letters</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Gañán, J.</au><au>Morante-Zarcero, S.</au><au>Pérez-Quintanilla, D.</au><au>Sierra, I.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Evaluation of mesoporous imprinted silicas as MSPD selective sorbents of ketoprofen in powder milk</atitle><jtitle>Materials letters</jtitle><date>2017-06-15</date><risdate>2017</risdate><volume>197</volume><spage>5</spage><epage>7</epage><pages>5-7</pages><issn>0167-577X</issn><eissn>1873-4979</eissn><abstract>•New mesoporous imprinted silicas were prepared using ketoprofen as template.•Materials were evaluated as sorbent in matrix solid phase dispersion for extraction of NSAIDs.•Results show that SBA-15-MIS-2 is appropriate to selective extraction of ketoprofen in powder milk.
Two molecularly imprinted mesoporous silicas were synthesized using different ratios of ketoprofen as template molecule and amino-functionalized SBA-15 as support. The materials synthesized were characterized and evaluated as selective sorbents for matrix solid phase dispersion (MSPD) of ketoprofen in the presence of other nonsteroidal anti-inflammatory drugs (NSAIDs) in powder milk samples.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/j.matlet.2017.03.137</doi><tpages>3</tpages></addata></record> |
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| source | Elsevier ScienceDirect Journals Complete |
| subjects | Chemical synthesis Imprinted mesoporous silica Ketoprofen Materials science Milk Molecular imprinting MSPD Nonsteroidal anti-inflammatory drugs NSAIDs Silica Sorbents |
| title | Evaluation of mesoporous imprinted silicas as MSPD selective sorbents of ketoprofen in powder milk |
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