Preparation of ZrB2-SiC ceramics by single-step and optimized two-step hot pressing using nanosized ZrB2 powders

•Nanosized ZrB2 powders were used to fabricate ZrB2-SiC ceramics.•High strength ZrB2-SiC ceramic was obtained by hot pressing at 1800°C.•An optimized two-step hot pressing method was designed for preparation of ZrB2-SiC ceramic at low temperature. ZrB2-SiC ceramics were prepared by single-step hot p...

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Veröffentlicht in:Materials letters 2017-08, Vol.200, p.14-17
Hauptverfasser: Hu, Ping, Gui, Kaixuan, Hong, Wenhu, Zhang, Xinghong
Format: Artikel
Sprache:eng
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Zusammenfassung:•Nanosized ZrB2 powders were used to fabricate ZrB2-SiC ceramics.•High strength ZrB2-SiC ceramic was obtained by hot pressing at 1800°C.•An optimized two-step hot pressing method was designed for preparation of ZrB2-SiC ceramic at low temperature. ZrB2-SiC ceramics were prepared by single-step hot pressing in the temperature range of 1500∼1800°C using nanosized ZrB2 powders. Dense ZrB2-SiC with high flexural strength (1044±79MPa) and fracture toughness (6.21±0.25MPa·m1/2) was obtained at 1800°C. An optimized two-step hot pressing process was designed and showed great advantages in fabricating of ZrB2-SiC ceramic with a high relative density (>98%) at low temperature. Furthermore, a high flexural strength (901±65MPa) was obtained, much higher than that of ZrB2-SiC (587±72MPa) by single-step hot pressing at the same sintering temperature.
ISSN:0167-577X
1873-4979
DOI:10.1016/j.matlet.2017.04.089