Novel (4-oxothiazolidine-2-ylidene)benzamide derivatives: synthesis, characterization and crystal structures

Novel (4-oxothiazolidine-2-ylidene)benzamide derivatives: synthesis, characterization and crystal structures

A convenient, one-pot, multicomponent synthesis of new (4-oxothiazolidine-2-ylidene)benzamide derivatives by unsymmetrical thioureas, various amines and methyl bromoacetate has been developed. These new compounds were characterized by IR, 1 HNMR, 13 CNMR, mass spectrometry, CHNS elemental analysis,...

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Veröffentlicht in:Research on chemical intermediates 2017-07, Vol.43 (7), p.4189-4199
Hauptverfasser: Hossaini, Mahshid, Heydari, Reza, Maghsoodlou, Malek Taher, Graiff, Claudia
Format: Artikel
Sprache:eng
Schlagworte:
Amines
Benzamide
Catalysis
Chemistry
Chemistry and Materials Science
Crystal structure
Derivatives
Infrared radiation
Infrared spectroscopy
Inorganic Chemistry
Mass spectrometry
Physical Chemistry
Single crystals
Thioureas
X ray analysis
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Beschreibung
Zusammenfassung:A convenient, one-pot, multicomponent synthesis of new (4-oxothiazolidine-2-ylidene)benzamide derivatives by unsymmetrical thioureas, various amines and methyl bromoacetate has been developed. These new compounds were characterized by IR, 1 HNMR, 13 CNMR, mass spectrometry, CHNS elemental analysis, and single-crystal X-ray analysis.
ISSN:0922-6168
1568-5675
DOI:10.1007/s11164-017-2872-0