Preparation and proton conductivity of ultrafine Y-doped BaZrO3 ceramics

Y-doped BaZrO3 powders prepared by high-temperature solid state reactions often suffer the disadvantage of serious aggregation. In order to eliminate this disadvantage, planet-mill and sand-mill processing methods were employed. The results of particle-size determination and scanning electron micros...

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Veröffentlicht in:Journal of the Ceramic Society of Japan 2017/06/01, Vol.125(6), pp.520-523
Hauptverfasser: YUANSHENG, Du, JINFENG, Xia, HONGQIANG, Nian, GUOHONG, Zhou, DANYU, Jiang, QIANG, Li
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container_end_page 523
container_issue 6
container_start_page 520
container_title Journal of the Ceramic Society of Japan
container_volume 125
creator YUANSHENG, Du
JINFENG, Xia
HONGQIANG, Nian
GUOHONG, Zhou
DANYU, Jiang
QIANG, Li
description Y-doped BaZrO3 powders prepared by high-temperature solid state reactions often suffer the disadvantage of serious aggregation. In order to eliminate this disadvantage, planet-mill and sand-mill processing methods were employed. The results of particle-size determination and scanning electron microscopy images confirm that sand milling can efficiently eliminate the aggregation and produce ultrafine and well-dispersed Y-doped BaZrO3 powders. Starting from powders treated by sand milling, completely densified Y-doped BaZrO3 ceramics can be fabricated by sintering at a low temperature of 1640°C for 15 h. Y-doped BaZrO3 ceramics sintered from powders treated by sand-mill for 5 h possess an ultrafine crystal size and a higher density and proton conductivity compared to those treated for 2 h.
doi_str_mv 10.2109/jcersj2.17017
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In order to eliminate this disadvantage, planet-mill and sand-mill processing methods were employed. The results of particle-size determination and scanning electron microscopy images confirm that sand milling can efficiently eliminate the aggregation and produce ultrafine and well-dispersed Y-doped BaZrO3 powders. Starting from powders treated by sand milling, completely densified Y-doped BaZrO3 ceramics can be fabricated by sintering at a low temperature of 1640°C for 15 h. 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subjects Agglomeration
Aggregation
Barium zirconates
Ceramic powders
Ceramics
Conductivity
Crystals
Density
Dispersion
Dispersions
Proton conductivity
Sand
Sand mill
Scanning electron microscopy
Sintering
Size determination
Solid state
Ultrafine ceramics
Y-doped BaZrO3
title Preparation and proton conductivity of ultrafine Y-doped BaZrO3 ceramics
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