Determination of isotopic composition of uranium samples using alpha spectrometry
Alpha spectrometry has been employed for the determination of the atom ratios of low enriched uranium samples. WinALPHA was used for the deconvolution and tail correction of the alpha spectra. The atom ratios calculated from alpha spectrometry were compared with that obtained by thermal ionisation m...
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| Veröffentlicht in: | Journal of radioanalytical and nuclear chemistry 2016-11, Vol.310 (2), p.541-546 |
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| container_title | Journal of radioanalytical and nuclear chemistry |
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| creator | Alamelu, D. Jagadish Kumar, S. |
| description | Alpha spectrometry has been employed for the determination of the atom ratios of low enriched uranium samples. WinALPHA was used for the deconvolution and tail correction of the alpha spectra. The atom ratios calculated from alpha spectrometry were compared with that obtained by thermal ionisation mass spectrometry. The results are in good agreement and is encouraging. The tail correction methodology WinALPHA is shown to be applicable for deconvoluting when the alpha activity of high energy peak is more than 45 times the lower energy peaks for obtaining the correct alpha activity ratio which is very challenging and been done for the first time. |
| doi_str_mv | 10.1007/s10967-016-4874-6 |
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WinALPHA was used for the deconvolution and tail correction of the alpha spectra. The atom ratios calculated from alpha spectrometry were compared with that obtained by thermal ionisation mass spectrometry. The results are in good agreement and is encouraging. The tail correction methodology WinALPHA is shown to be applicable for deconvoluting when the alpha activity of high energy peak is more than 45 times the lower energy peaks for obtaining the correct alpha activity ratio which is very challenging and been done for the first time.</description><identifier>ISSN: 0236-5731</identifier><identifier>EISSN: 1588-2780</identifier><identifier>DOI: 10.1007/s10967-016-4874-6</identifier><language>eng</language><publisher>Dordrecht: Springer Netherlands</publisher><subject>Chemistry ; Chemistry and Materials Science ; Comparative analysis ; Diagnostic Radiology ; Enriched uranium ; Hadrons ; Heavy Ions ; Inorganic Chemistry ; Ionization ; Isotopes ; Mass spectrometry ; Nuclear Chemistry ; Nuclear Physics ; Physical Chemistry ; Scientific imaging ; Spectroscopy ; Uranium</subject><ispartof>Journal of radioanalytical and nuclear chemistry, 2016-11, Vol.310 (2), p.541-546</ispartof><rights>Akadémiai Kiadó, Budapest, Hungary 2016</rights><rights>COPYRIGHT 2016 Springer</rights><rights>Copyright Springer Science & Business Media 2016</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c355t-b507839e95716a0f73694cee81e6133cdd63df77c6061e74b4a26530a22f62cc3</citedby><cites>FETCH-LOGICAL-c355t-b507839e95716a0f73694cee81e6133cdd63df77c6061e74b4a26530a22f62cc3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10967-016-4874-6$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10967-016-4874-6$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Alamelu, D.</creatorcontrib><creatorcontrib>Jagadish Kumar, S.</creatorcontrib><title>Determination of isotopic composition of uranium samples using alpha spectrometry</title><title>Journal of radioanalytical and nuclear chemistry</title><addtitle>J Radioanal Nucl Chem</addtitle><description>Alpha spectrometry has been employed for the determination of the atom ratios of low enriched uranium samples. WinALPHA was used for the deconvolution and tail correction of the alpha spectra. The atom ratios calculated from alpha spectrometry were compared with that obtained by thermal ionisation mass spectrometry. The results are in good agreement and is encouraging. The tail correction methodology WinALPHA is shown to be applicable for deconvoluting when the alpha activity of high energy peak is more than 45 times the lower energy peaks for obtaining the correct alpha activity ratio which is very challenging and been done for the first time.</description><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Comparative analysis</subject><subject>Diagnostic Radiology</subject><subject>Enriched uranium</subject><subject>Hadrons</subject><subject>Heavy Ions</subject><subject>Inorganic Chemistry</subject><subject>Ionization</subject><subject>Isotopes</subject><subject>Mass spectrometry</subject><subject>Nuclear Chemistry</subject><subject>Nuclear Physics</subject><subject>Physical Chemistry</subject><subject>Scientific imaging</subject><subject>Spectroscopy</subject><subject>Uranium</subject><issn>0236-5731</issn><issn>1588-2780</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><recordid>eNp1kE1LxDAQhoMouK7-AG8Fz9VJ03z0uKyfsCCCnkM2na5Z2qYm6WH_vV2q4EXmMDC8z8zwEHJN4ZYCyLtIoRIyByryUskyFydkQblSeSEVnJIFFEzkXDJ6Ti5i3ANApRRbkLd7TBg615vkfJ_5JnPRJz84m1nfDT663_kYTO_GLoumG1qM2Rhdv8tMO3yaLA5oU_AdpnC4JGeNaSNe_fQl-Xh8eF8_55vXp5f1apNbxnnKtxykYhVWXFJhoJFMVKVFVBQFZczWtWB1I6UVICjKcluaQnAGpigaUVjLluRm3jsE_zViTHrvx9BPJzVVCpRgkhZT6nZO7UyL2vWNT8HYqWrsnPU9Nm6ar0oJkvIK-ATQGbDBxxiw0UNwnQkHTUEfVetZtZ5U66NqLSammJk4Zfsdhj-v_At9A11dgWk</recordid><startdate>20161101</startdate><enddate>20161101</enddate><creator>Alamelu, D.</creator><creator>Jagadish Kumar, S.</creator><general>Springer Netherlands</general><general>Springer</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20161101</creationdate><title>Determination of isotopic composition of uranium samples using alpha spectrometry</title><author>Alamelu, D. ; Jagadish Kumar, S.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c355t-b507839e95716a0f73694cee81e6133cdd63df77c6061e74b4a26530a22f62cc3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2016</creationdate><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Comparative analysis</topic><topic>Diagnostic Radiology</topic><topic>Enriched uranium</topic><topic>Hadrons</topic><topic>Heavy Ions</topic><topic>Inorganic Chemistry</topic><topic>Ionization</topic><topic>Isotopes</topic><topic>Mass spectrometry</topic><topic>Nuclear Chemistry</topic><topic>Nuclear Physics</topic><topic>Physical Chemistry</topic><topic>Scientific imaging</topic><topic>Spectroscopy</topic><topic>Uranium</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Alamelu, D.</creatorcontrib><creatorcontrib>Jagadish Kumar, S.</creatorcontrib><collection>CrossRef</collection><jtitle>Journal of radioanalytical and nuclear chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Alamelu, D.</au><au>Jagadish Kumar, S.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Determination of isotopic composition of uranium samples using alpha spectrometry</atitle><jtitle>Journal of radioanalytical and nuclear chemistry</jtitle><stitle>J Radioanal Nucl Chem</stitle><date>2016-11-01</date><risdate>2016</risdate><volume>310</volume><issue>2</issue><spage>541</spage><epage>546</epage><pages>541-546</pages><issn>0236-5731</issn><eissn>1588-2780</eissn><abstract>Alpha spectrometry has been employed for the determination of the atom ratios of low enriched uranium samples. WinALPHA was used for the deconvolution and tail correction of the alpha spectra. The atom ratios calculated from alpha spectrometry were compared with that obtained by thermal ionisation mass spectrometry. The results are in good agreement and is encouraging. The tail correction methodology WinALPHA is shown to be applicable for deconvoluting when the alpha activity of high energy peak is more than 45 times the lower energy peaks for obtaining the correct alpha activity ratio which is very challenging and been done for the first time.</abstract><cop>Dordrecht</cop><pub>Springer Netherlands</pub><doi>10.1007/s10967-016-4874-6</doi><tpages>6</tpages></addata></record> |
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| subjects | Chemistry Chemistry and Materials Science Comparative analysis Diagnostic Radiology Enriched uranium Hadrons Heavy Ions Inorganic Chemistry Ionization Isotopes Mass spectrometry Nuclear Chemistry Nuclear Physics Physical Chemistry Scientific imaging Spectroscopy Uranium |
| title | Determination of isotopic composition of uranium samples using alpha spectrometry |
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