Crystal structure of the complex of copper(II) with 3-(2-hydroxy-3-sulfo-5-nitrophenylazo)-pentadione-2,4
A new complex of copper (II) with 3-(2-hydroxy-3-sulfo-5-nitrophenylazo)-pentadione-2,4 (HL) is synthesized and analyzed by single crystal XRD. The crystals are monoclinic: a = 7.7563(4) Å, b = 24.0157(12) Å, c = 24.6353(13) Å, β = 91.9490(10)°, V = 4586.2(4) Å 3 , space group P2 1 / c , Z = 2, ρ ca...
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| Veröffentlicht in: | Journal of structural chemistry 2016-07, Vol.57 (4), p.819-821 |
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| container_issue | 4 |
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| container_title | Journal of structural chemistry |
| container_volume | 57 |
| creator | Maharramov, A. M. Alieva, R. A. Nazarova, G. G. Bakhmanova, F. N. Askerov, R. K. Chyragov, F. M. |
| description | A new complex of copper (II) with 3-(2-hydroxy-3-sulfo-5-nitrophenylazo)-pentadione-2,4 (HL) is synthesized and analyzed by single crystal XRD. The crystals are monoclinic:
a
= 7.7563(4) Å,
b
= 24.0157(12) Å,
c
= 24.6353(13) Å, β = 91.9490(10)°,
V
= 4586.2(4) Å
3
, space group P2
1
/
c
,
Z
= 2, ρ
calc
= 1.713 g/cm
3
,
R
= 0.0695. The environment of the copper atom is formed by three oxygen atoms, the nitrogen atom of tetradentate ligand, and the oxygen atom of a water molecule. |
| doi_str_mv | 10.1134/S0022476616040296 |
| format | Article |
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a
= 7.7563(4) Å,
b
= 24.0157(12) Å,
c
= 24.6353(13) Å, β = 91.9490(10)°,
V
= 4586.2(4) Å
3
, space group P2
1
/
c
,
Z
= 2, ρ
calc
= 1.713 g/cm
3
,
R
= 0.0695. The environment of the copper atom is formed by three oxygen atoms, the nitrogen atom of tetradentate ligand, and the oxygen atom of a water molecule.</description><identifier>ISSN: 0022-4766</identifier><identifier>EISSN: 1573-8779</identifier><identifier>DOI: 10.1134/S0022476616040296</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Atomic ; Atomic/Molecular Structure and Spectra ; Brief Communications ; Chemistry ; Chemistry and Materials Science ; Copper ; Crystal structure ; Inorganic Chemistry ; Molecular ; Optical and Plasma Physics ; Oxygen atoms ; Physical Chemistry ; Single crystals ; Solid State Physics</subject><ispartof>Journal of structural chemistry, 2016-07, Vol.57 (4), p.819-821</ispartof><rights>Pleiades Publishing, Ltd. 2016</rights><rights>Copyright Springer Science & Business Media 2016</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c316t-657d6c0733a7c5f33efbd8d394be9453c6a61aae4fe1e9ff7354258f509f1cef3</citedby><cites>FETCH-LOGICAL-c316t-657d6c0733a7c5f33efbd8d394be9453c6a61aae4fe1e9ff7354258f509f1cef3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S0022476616040296$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S0022476616040296$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Maharramov, A. M.</creatorcontrib><creatorcontrib>Alieva, R. A.</creatorcontrib><creatorcontrib>Nazarova, G. G.</creatorcontrib><creatorcontrib>Bakhmanova, F. N.</creatorcontrib><creatorcontrib>Askerov, R. K.</creatorcontrib><creatorcontrib>Chyragov, F. M.</creatorcontrib><title>Crystal structure of the complex of copper(II) with 3-(2-hydroxy-3-sulfo-5-nitrophenylazo)-pentadione-2,4</title><title>Journal of structural chemistry</title><addtitle>J Struct Chem</addtitle><description>A new complex of copper (II) with 3-(2-hydroxy-3-sulfo-5-nitrophenylazo)-pentadione-2,4 (HL) is synthesized and analyzed by single crystal XRD. The crystals are monoclinic:
a
= 7.7563(4) Å,
b
= 24.0157(12) Å,
c
= 24.6353(13) Å, β = 91.9490(10)°,
V
= 4586.2(4) Å
3
, space group P2
1
/
c
,
Z
= 2, ρ
calc
= 1.713 g/cm
3
,
R
= 0.0695. The environment of the copper atom is formed by three oxygen atoms, the nitrogen atom of tetradentate ligand, and the oxygen atom of a water molecule.</description><subject>Atomic</subject><subject>Atomic/Molecular Structure and Spectra</subject><subject>Brief Communications</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Copper</subject><subject>Crystal structure</subject><subject>Inorganic Chemistry</subject><subject>Molecular</subject><subject>Optical and Plasma Physics</subject><subject>Oxygen atoms</subject><subject>Physical Chemistry</subject><subject>Single crystals</subject><subject>Solid State Physics</subject><issn>0022-4766</issn><issn>1573-8779</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><recordid>eNp1kF1LwzAYhYMoOKc_wLuCNxsYzUebNJcy_BgMvFCvS5a-cR1dU5MUV3-9LfNCEK9eDuc854WD0CUlN5Ty9PaFEMZSKQQVJCVMiSM0oZnkOJdSHaPJaOPRP0VnIWwJISpXYoKqhe9D1HUSou9M7DwkziZxA4lxu7aG_SiNa1vws-VynnxWcZNwPGN405fe7XvMcehq63CGmyp6126g6Wv95ea4hSbqsnINYHadnqMTq-sAFz93it4e7l8XT3j1_Lhc3K2w4VRELDJZCkMk51qazHIOdl3mJVfpGlSacSO0oFpDaoGCslbyLGVZbjOiLDVg-RRdHXpb7z46CLHYus43w8uC5jnJBeeKDSl6SBnvQvBgi9ZXO-37gpJiXLT4s-jAsAMThmzzDv5X87_QN8gSd0w</recordid><startdate>20160701</startdate><enddate>20160701</enddate><creator>Maharramov, A. M.</creator><creator>Alieva, R. A.</creator><creator>Nazarova, G. G.</creator><creator>Bakhmanova, F. N.</creator><creator>Askerov, R. K.</creator><creator>Chyragov, F. M.</creator><general>Pleiades Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20160701</creationdate><title>Crystal structure of the complex of copper(II) with 3-(2-hydroxy-3-sulfo-5-nitrophenylazo)-pentadione-2,4</title><author>Maharramov, A. M. ; Alieva, R. A. ; Nazarova, G. G. ; Bakhmanova, F. N. ; Askerov, R. K. ; Chyragov, F. M.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c316t-657d6c0733a7c5f33efbd8d394be9453c6a61aae4fe1e9ff7354258f509f1cef3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2016</creationdate><topic>Atomic</topic><topic>Atomic/Molecular Structure and Spectra</topic><topic>Brief Communications</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Copper</topic><topic>Crystal structure</topic><topic>Inorganic Chemistry</topic><topic>Molecular</topic><topic>Optical and Plasma Physics</topic><topic>Oxygen atoms</topic><topic>Physical Chemistry</topic><topic>Single crystals</topic><topic>Solid State Physics</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Maharramov, A. M.</creatorcontrib><creatorcontrib>Alieva, R. A.</creatorcontrib><creatorcontrib>Nazarova, G. G.</creatorcontrib><creatorcontrib>Bakhmanova, F. N.</creatorcontrib><creatorcontrib>Askerov, R. K.</creatorcontrib><creatorcontrib>Chyragov, F. M.</creatorcontrib><collection>CrossRef</collection><jtitle>Journal of structural chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Maharramov, A. M.</au><au>Alieva, R. A.</au><au>Nazarova, G. G.</au><au>Bakhmanova, F. N.</au><au>Askerov, R. K.</au><au>Chyragov, F. M.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Crystal structure of the complex of copper(II) with 3-(2-hydroxy-3-sulfo-5-nitrophenylazo)-pentadione-2,4</atitle><jtitle>Journal of structural chemistry</jtitle><stitle>J Struct Chem</stitle><date>2016-07-01</date><risdate>2016</risdate><volume>57</volume><issue>4</issue><spage>819</spage><epage>821</epage><pages>819-821</pages><issn>0022-4766</issn><eissn>1573-8779</eissn><abstract>A new complex of copper (II) with 3-(2-hydroxy-3-sulfo-5-nitrophenylazo)-pentadione-2,4 (HL) is synthesized and analyzed by single crystal XRD. The crystals are monoclinic:
a
= 7.7563(4) Å,
b
= 24.0157(12) Å,
c
= 24.6353(13) Å, β = 91.9490(10)°,
V
= 4586.2(4) Å
3
, space group P2
1
/
c
,
Z
= 2, ρ
calc
= 1.713 g/cm
3
,
R
= 0.0695. The environment of the copper atom is formed by three oxygen atoms, the nitrogen atom of tetradentate ligand, and the oxygen atom of a water molecule.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S0022476616040296</doi><tpages>3</tpages></addata></record> |
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| subjects | Atomic Atomic/Molecular Structure and Spectra Brief Communications Chemistry Chemistry and Materials Science Copper Crystal structure Inorganic Chemistry Molecular Optical and Plasma Physics Oxygen atoms Physical Chemistry Single crystals Solid State Physics |
| title | Crystal structure of the complex of copper(II) with 3-(2-hydroxy-3-sulfo-5-nitrophenylazo)-pentadione-2,4 |
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