Achievement of 1H–19F heteronuclear experiments using the conventional spectrometer with a shared single high band amplifier
The 1H–19F heteronuclear NMR experiments were achieved using the conventional spectrometer equipped with a single high band amplifier and a 1H/19F/13C double‐tuned probe. Although double high band amplifiers are generally required to perform such experiments, a simple modification of pathway in the...
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Veröffentlicht in: | Magnetic resonance in chemistry 2015-05, Vol.53 (5), p.327-329 |
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Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | The 1H–19F heteronuclear NMR experiments were achieved using the conventional spectrometer equipped with a single high band amplifier and a 1H/19F/13C double‐tuned probe. Although double high band amplifiers are generally required to perform such experiments, a simple modification of pathway in the conventional spectrometer was capable of acquiring various 1H–19F heteronuclear spectra. The efficiency of the present technique was demonstrated in an application for 19F{1H} and 1H{19F} saturation transfer difference experiments. Copyright © 2015 John Wiley & Sons, Ltd.
The 1H‐19F heteronuclear NMR experiments were achieved using the conventional spectrometer equipped with a single high band amplifier and a 1H/19F/13C‐double tuned probe. Although double high band amplifiers are generally required to perform such experiments, a simple modification of pathway in the conventional spectrometer was capable of acquiring various 1H‐19F heteronuclear spectra. |
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ISSN: | 0749-1581 1097-458X |
DOI: | 10.1002/mrc.4210 |