Achievement of 1H–19F heteronuclear experiments using the conventional spectrometer with a shared single high band amplifier

The 1H–19F heteronuclear NMR experiments were achieved using the conventional spectrometer equipped with a single high band amplifier and a 1H/19F/13C double‐tuned probe. Although double high band amplifiers are generally required to perform such experiments, a simple modification of pathway in the...

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Veröffentlicht in:Magnetic resonance in chemistry 2015-05, Vol.53 (5), p.327-329
Hauptverfasser: Sakuma, Chiseko, Kurita, Jun‐ichi, Furihata, Kazuo, Tashiro, Mitsuru
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Sprache:eng
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Zusammenfassung:The 1H–19F heteronuclear NMR experiments were achieved using the conventional spectrometer equipped with a single high band amplifier and a 1H/19F/13C double‐tuned probe. Although double high band amplifiers are generally required to perform such experiments, a simple modification of pathway in the conventional spectrometer was capable of acquiring various 1H–19F heteronuclear spectra. The efficiency of the present technique was demonstrated in an application for 19F{1H} and 1H{19F} saturation transfer difference experiments. Copyright © 2015 John Wiley & Sons, Ltd. The 1H‐19F heteronuclear NMR experiments were achieved using the conventional spectrometer equipped with a single high band amplifier and a 1H/19F/13C‐double tuned probe. Although double high band amplifiers are generally required to perform such experiments, a simple modification of pathway in the conventional spectrometer was capable of acquiring various 1H‐19F heteronuclear spectra.
ISSN:0749-1581
1097-458X
DOI:10.1002/mrc.4210