N-Nitrosation of Secondary Amines Using Supported Perchloric Acid on Silica Gel and Stereoselectivity Study of Nitrosated Products

N-Nitrosation of Secondary Amines Using Supported Perchloric Acid on Silica Gel and Stereoselectivity Study of Nitrosated Products

N‐Nitrosation of different types of secondary amines has been proceeded using supported perchloric acid on silica gel and sodiume nitrite under heterogeneous conditions. The operational system is simple and high pure products can be easily isolated with good to high yields. N‐Nitrosation of differen...

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Veröffentlicht in:Journal of the Chinese Chemical Society (Taipei) 2013-10, Vol.60 (10), p.1272-1276
Hauptverfasser: Goudarziafshar, Hamid, Ghorbani-Choghamarani, Arash, Hadian, Laila
Format: Artikel
Sprache:eng
Schlagworte:
Chemical industry
Heterogeneous
N-Nitrosation
Perchloric acid
Secondary amines
Silica
Sodium nitrite
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Beschreibung
Zusammenfassung:N‐Nitrosation of different types of secondary amines has been proceeded using supported perchloric acid on silica gel and sodiume nitrite under heterogeneous conditions. The operational system is simple and high pure products can be easily isolated with good to high yields. N‐Nitrosation of different types of secondary amines has been carried out using HClO4‐SiO2 and NaNO2 under heterogeneous conditions.
ISSN:0009-4536
2192-6549
DOI:10.1002/jccs.201300136