A Solvent-free Synthesis of Zn–Al Layered Double Hydroxides

We have demonstrated for the first time a solvent-free synthesis of Zn–Al layered double hydroxides, Zn–Al LDH(Cl), by grinding solid ZnO and AlCl3·6H2O and then by autoclaving at 150 °C for 1 day without the addition of water and alkaline solution.

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Veröffentlicht in:Chemistry letters 2007-03, Vol.36 (3), p.446-447
Hauptverfasser: Chitrakar, Ramesh, Tezuka, Satoko, Sonoda, Akinari, Sakane, Kohji, Ooi, Kenta, Hirotsu, Takahiro
Format: Artikel
Sprache:eng
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Zusammenfassung:We have demonstrated for the first time a solvent-free synthesis of Zn–Al layered double hydroxides, Zn–Al LDH(Cl), by grinding solid ZnO and AlCl3·6H2O and then by autoclaving at 150 °C for 1 day without the addition of water and alkaline solution.
ISSN:0366-7022
1348-0715
DOI:10.1246/cl.2007.446