Analysis of Mixed Drugs by Mass Spectrometry, VIII
Although in previous paper, we reported that mass spectrum of sulpyrine(I), sodium methan sulfonate of monomethylaminoantipyrine(III), is diffcult to measure due to its non-volatility. It was found that reproducible mass spectrum of thermal degraduation products of sulpyrine was obtained by raising...
Gespeichert in:
| Veröffentlicht in: | Journal of the Mass Spectrometry Society of Japan 1967/12/31, Vol.15(3-4), pp.198-203 |
|---|---|
| Hauptverfasser: | , , |
| Format: | Artikel |
| Sprache: | eng |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 203 |
|---|---|
| container_issue | 3-4 |
| container_start_page | 198 |
| container_title | Journal of the Mass Spectrometry Society of Japan |
| container_volume | 15 |
| creator | TATEMATSU, AKIRA YOSIZUMI, HIDEO GOTO, TOSHIO |
| description | Although in previous paper, we reported that mass spectrum of sulpyrine(I), sodium methan sulfonate of monomethylaminoantipyrine(III), is diffcult to measure due to its non-volatility. It was found that reproducible mass spectrum of thermal degraduation products of sulpyrine was obtained by raising temperature of ionization chamber and of heated inlet-system to about 250°. The identification of sulpyrine in the various preparations, (powder, granule, tablet, and injection etc.) containing sulpyrine by examination of their mass spectra is thus possible. By comparison of mass spectra of 4 kinds of pyrazolone derivatives, fragmentation of sulpyrine was also discussed. |
| doi_str_mv | 10.5702/massspec1953.15.198 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_1446898576</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>3112150861</sourcerecordid><originalsourceid>FETCH-LOGICAL-c2438-36b3267579e0d871b884c26164e315359d94a677cae60c994ebfb276959faabc3</originalsourceid><addsrcrecordid>eNplkEtLAzEUhYMoWKu_wE3ArVPzfixLtTrQ4sLHNmTSTJ3SdmruFJx_b6RSBFfnLs537uEgdE3JSGrC7jYeAHYxUCv5iMoRteYEDagxpBCMydN8c0EKQ6w-RxcAK0IEU1oPEBtv_bqHBnBb43nzFRf4Pu2XgKsez3MqfsmxXWo3sUv9LX4vy_ISndV-DfHqV4fobfrwOnkqZs-P5WQ8KwIT3BRcVTz_kNpGsjCaVsaIwBRVInIqubQLK3zuEHxUJFgrYlVXTCsrbe19FfgQ3Rxyd6n93Efo3Krdp1wXHBVCGWukVtnFD66QWoAUa7dLzcan3lHifsZxf8dxVLo8TqZmB2oFnV_GI-NT14R1_MdwJ45izdEWPnxyccu_AWpHcro</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1446898576</pqid></control><display><type>article</type><title>Analysis of Mixed Drugs by Mass Spectrometry, VIII</title><source>Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals</source><source>J-STAGE (Japan Science & Technology Information Aggregator, Electronic) Freely Available Titles - Japanese</source><source>Free Full-Text Journals in Chemistry</source><creator>TATEMATSU, AKIRA ; YOSIZUMI, HIDEO ; GOTO, TOSHIO</creator><creatorcontrib>TATEMATSU, AKIRA ; YOSIZUMI, HIDEO ; GOTO, TOSHIO</creatorcontrib><description>Although in previous paper, we reported that mass spectrum of sulpyrine(I), sodium methan sulfonate of monomethylaminoantipyrine(III), is diffcult to measure due to its non-volatility. It was found that reproducible mass spectrum of thermal degraduation products of sulpyrine was obtained by raising temperature of ionization chamber and of heated inlet-system to about 250°. The identification of sulpyrine in the various preparations, (powder, granule, tablet, and injection etc.) containing sulpyrine by examination of their mass spectra is thus possible. By comparison of mass spectra of 4 kinds of pyrazolone derivatives, fragmentation of sulpyrine was also discussed.</description><identifier>ISSN: 1340-8097</identifier><identifier>EISSN: 1880-4225</identifier><identifier>EISSN: 1884-3271</identifier><identifier>DOI: 10.5702/massspec1953.15.198</identifier><language>eng</language><publisher>Tokyo: The Mass Spectrometry Society of Japan</publisher><ispartof>Journal of the Mass Spectrometry Society of Japan, 1967/12/31, Vol.15(3-4), pp.198-203</ispartof><rights>The Mass Spectrometry Society of Japan</rights><rights>Copyright Japan Science and Technology Agency 1967</rights><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,1883,4024,27923,27924,27925</link.rule.ids></links><search><creatorcontrib>TATEMATSU, AKIRA</creatorcontrib><creatorcontrib>YOSIZUMI, HIDEO</creatorcontrib><creatorcontrib>GOTO, TOSHIO</creatorcontrib><title>Analysis of Mixed Drugs by Mass Spectrometry, VIII</title><title>Journal of the Mass Spectrometry Society of Japan</title><addtitle>J. Mass Spectrom. Soc. Jpn.</addtitle><description>Although in previous paper, we reported that mass spectrum of sulpyrine(I), sodium methan sulfonate of monomethylaminoantipyrine(III), is diffcult to measure due to its non-volatility. It was found that reproducible mass spectrum of thermal degraduation products of sulpyrine was obtained by raising temperature of ionization chamber and of heated inlet-system to about 250°. The identification of sulpyrine in the various preparations, (powder, granule, tablet, and injection etc.) containing sulpyrine by examination of their mass spectra is thus possible. By comparison of mass spectra of 4 kinds of pyrazolone derivatives, fragmentation of sulpyrine was also discussed.</description><issn>1340-8097</issn><issn>1880-4225</issn><issn>1884-3271</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1967</creationdate><recordtype>article</recordtype><recordid>eNplkEtLAzEUhYMoWKu_wE3ArVPzfixLtTrQ4sLHNmTSTJ3SdmruFJx_b6RSBFfnLs537uEgdE3JSGrC7jYeAHYxUCv5iMoRteYEDagxpBCMydN8c0EKQ6w-RxcAK0IEU1oPEBtv_bqHBnBb43nzFRf4Pu2XgKsez3MqfsmxXWo3sUv9LX4vy_ISndV-DfHqV4fobfrwOnkqZs-P5WQ8KwIT3BRcVTz_kNpGsjCaVsaIwBRVInIqubQLK3zuEHxUJFgrYlVXTCsrbe19FfgQ3Rxyd6n93Efo3Krdp1wXHBVCGWukVtnFD66QWoAUa7dLzcan3lHifsZxf8dxVLo8TqZmB2oFnV_GI-NT14R1_MdwJ45izdEWPnxyccu_AWpHcro</recordid><startdate>1967</startdate><enddate>1967</enddate><creator>TATEMATSU, AKIRA</creator><creator>YOSIZUMI, HIDEO</creator><creator>GOTO, TOSHIO</creator><general>The Mass Spectrometry Society of Japan</general><general>Japan Science and Technology Agency</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope></search><sort><creationdate>1967</creationdate><title>Analysis of Mixed Drugs by Mass Spectrometry, VIII</title><author>TATEMATSU, AKIRA ; YOSIZUMI, HIDEO ; GOTO, TOSHIO</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c2438-36b3267579e0d871b884c26164e315359d94a677cae60c994ebfb276959faabc3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1967</creationdate><toplevel>online_resources</toplevel><creatorcontrib>TATEMATSU, AKIRA</creatorcontrib><creatorcontrib>YOSIZUMI, HIDEO</creatorcontrib><creatorcontrib>GOTO, TOSHIO</creatorcontrib><collection>CrossRef</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of the Mass Spectrometry Society of Japan</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>TATEMATSU, AKIRA</au><au>YOSIZUMI, HIDEO</au><au>GOTO, TOSHIO</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Analysis of Mixed Drugs by Mass Spectrometry, VIII</atitle><jtitle>Journal of the Mass Spectrometry Society of Japan</jtitle><addtitle>J. Mass Spectrom. Soc. Jpn.</addtitle><date>1967</date><risdate>1967</risdate><volume>15</volume><issue>3-4</issue><spage>198</spage><epage>203</epage><pages>198-203</pages><issn>1340-8097</issn><eissn>1880-4225</eissn><eissn>1884-3271</eissn><abstract>Although in previous paper, we reported that mass spectrum of sulpyrine(I), sodium methan sulfonate of monomethylaminoantipyrine(III), is diffcult to measure due to its non-volatility. It was found that reproducible mass spectrum of thermal degraduation products of sulpyrine was obtained by raising temperature of ionization chamber and of heated inlet-system to about 250°. The identification of sulpyrine in the various preparations, (powder, granule, tablet, and injection etc.) containing sulpyrine by examination of their mass spectra is thus possible. By comparison of mass spectra of 4 kinds of pyrazolone derivatives, fragmentation of sulpyrine was also discussed.</abstract><cop>Tokyo</cop><pub>The Mass Spectrometry Society of Japan</pub><doi>10.5702/massspec1953.15.198</doi><tpages>6</tpages><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1340-8097 |
| ispartof | Journal of the Mass Spectrometry Society of Japan, 1967/12/31, Vol.15(3-4), pp.198-203 |
| issn | 1340-8097 1880-4225 1884-3271 |
| language | eng |
| recordid | cdi_proquest_journals_1446898576 |
| source | Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals; J-STAGE (Japan Science & Technology Information Aggregator, Electronic) Freely Available Titles - Japanese; Free Full-Text Journals in Chemistry |
| title | Analysis of Mixed Drugs by Mass Spectrometry, VIII |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-04T02%3A03%3A36IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Analysis%20of%20Mixed%20Drugs%20by%20Mass%20Spectrometry,%20VIII&rft.jtitle=Journal%20of%20the%20Mass%20Spectrometry%20Society%20of%20Japan&rft.au=TATEMATSU,%20AKIRA&rft.date=1967&rft.volume=15&rft.issue=3-4&rft.spage=198&rft.epage=203&rft.pages=198-203&rft.issn=1340-8097&rft.eissn=1880-4225&rft_id=info:doi/10.5702/massspec1953.15.198&rft_dat=%3Cproquest_cross%3E3112150861%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=1446898576&rft_id=info:pmid/&rfr_iscdi=true |