Identification Tests of Aristolochic Acid in Crude Drugs by Reversed-Phase TLC/Scanning Densitometry
We performed identification tests of aristolochic acid in Xixin, Mutong, Muxiang, and Fangji by reversed-phase TLC/scanning densitometry using aristolochic acid I as a marker compound. The developing solvents used were: I) acetonitrile/methanol/water mixture solution (3 : 1 : 1) and II) 2-butanone/m...
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Veröffentlicht in: | Journal of Health Science 2006, Vol.52(1), pp.78-81 |
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Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | We performed identification tests of aristolochic acid in Xixin, Mutong, Muxiang, and Fangji by reversed-phase TLC/scanning densitometry using aristolochic acid I as a marker compound. The developing solvents used were: I) acetonitrile/methanol/water mixture solution (3 : 1 : 1) and II) 2-butanone/methanol/sodium sulfate(1→20) mixture solution (2 : 1 : 1). The Rf value of aristolochic acid I was 0.54 using the I system and 0.57 using the II system. The maximum absorption wavelengths of aristolochic acid I observed by scanning densitometry were 254 and 325 nm. |
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ISSN: | 1344-9702 1347-5207 |
DOI: | 10.1248/jhs.52.78 |