Crystal Structure of Metformin·ethyl N-(3-tossulfonyl)carbamate

The title compound, C14H24N6O4S, was prepared by the reaction of ethyl N-(3-tossulfonyl)carbamate with metformin. It was crystallized in the triclinic system, space group P1 with a = 6.894(3)Å, b = 8.323(4)Å, c = 17.184(8)Å, α = 84.119(7)°, β = 84.028(6)°, γ = 75.479(6)°, V = 946.4(7)Å3, Z = 2, R =...

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Veröffentlicht in:	Analytical Sciences ; X-ray Structure and Analysis Online 2008, Vol.24, pp.x289-x290
Hauptverfasser:	HUANG, Liang, XI, Pin-xian, XU, Min, LIU, Tong-huan, ZENG, Zheng-zhi
Format:	Artikel
Sprache:	eng
Online-Zugang:	Volltext
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Beschreibung
Zusammenfassung:	The title compound, C14H24N6O4S, was prepared by the reaction of ethyl N-(3-tossulfonyl)carbamate with metformin. It was crystallized in the triclinic system, space group P1 with a = 6.894(3)Å, b = 8.323(4)Å, c = 17.184(8)Å, α = 84.119(7)°, β = 84.028(6)°, γ = 75.479(6)°, V = 946.4(7)Å3, Z = 2, R = 0.0426. The molecules are linked by two kinds of hydrogen-bonds, N-H…N and N-H…O, generating an extended two-dimensional supramolecular network structure in the ab plane.
ISSN:	1348-2238 1348-2238 1883-3578
DOI:	10.2116/analscix.24.x289