Two-dimensional INADEQUATE 13C NMR Study on Vitamin D3

Two-dimensional INADEQUATE 13C NMR Study on Vitamin D3

Two‐dimensional INADEQUATE 13C NMR spectroscopy has been used to find the carbon‐carbon connectivities of the carbon skeleton of vitamin D3. This information leads to the unambiguous assignment of the chemical shifts of all 27 carbon atoms of vitamin D3.

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Veröffentlicht in:Magnetic resonance in chemistry 1985-04, Vol.23 (4), p.267-270
Hauptverfasser: Kruk, C., Jans, A. W. H., Lugtenburg, J.
Format: Artikel
Sprache:eng
Schlagworte:
Analytical, structural and metabolic biochemistry
Biological and medical sciences
Coenzymes, vitamins
Fundamental and applied biological sciences. Psychology
Other biological molecules
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Zusammenfassung:Two‐dimensional INADEQUATE 13C NMR spectroscopy has been used to find the carbon‐carbon connectivities of the carbon skeleton of vitamin D3. This information leads to the unambiguous assignment of the chemical shifts of all 27 carbon atoms of vitamin D3.
ISSN:0749-1581
1097-458X
DOI:10.1002/mrc.1260230412