Synthesis and spectroscopic characterisation of 3-chloroperbenzoic acid-17O,18O, nitrosobenzene-17O,18O and nitrosobenzene-15N

3‐Chloroperbenzoic acid‐17O,18O was prepared from 3‐chlorobenzoyl chloride and hydrogen peroxide‐17O,18O (obtained by subjecting water‐17O,18O. Nitrobenzene‐15N was reduced to aniline‐15N, which was oxidised by 3‐chloroperbenzoic acid to nitrosobenzene‐15N. 15N and 17O NMR data are given for the cor...

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Veröffentlicht in:	Journal of labelled compounds & radiopharmaceuticals 1993-08, Vol.33 (8), p.739-746
Hauptverfasser:	Bleasdale, Christine, Ellis, Martin K., Farmer, Peter B., Golding, Bernard T., Handley, Kevin F., Jones, Peter, McFarlane, William
Format:	Artikel
Sprache:	eng
Schlagworte:	15N-labelling 17O-labelling 3-chloroperbenzoic acid Chemistry Exact sciences and technology Nitrosobenzene Noncondensed benzenic compounds Organic chemistry Preparations and properties
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Zusammenfassung:	3‐Chloroperbenzoic acid‐17O,18O was prepared from 3‐chlorobenzoyl chloride and hydrogen peroxide‐17O,18O (obtained by subjecting water‐17O,18O. Nitrobenzene‐15N was reduced to aniline‐15N, which was oxidised by 3‐chloroperbenzoic acid to nitrosobenzene‐15N. 15N and 17O NMR data are given for the corresponding labelled nitrosobenzene.
ISSN:	0362-4803 1099-1344
DOI:	10.1002/jlcr.2580330810