Revised 13C Nmr Assignments for Norditerpenoid Alkaloids with 7,8-Methylenedioxy and 10β-OH Groups
13C-nmr chemical shift assignments for the norditerpenoid alkaloids deltaline [1], deltamine [2], dictyocarpine [3], and 14-acetyldictyocarpine [5] have been revised on the basis of a study of their 1D, 2D, and selective INEPT nmr spectra. These revisions suggest that the 13C-nmr chemical shift assi...
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Veröffentlicht in: | Journal of natural products (Washington, D.C.) D.C.), 1993-07, Vol.56 (7), p.1140-1147 |
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Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | 13C-nmr chemical shift assignments for the norditerpenoid alkaloids deltaline [1], deltamine [2], dictyocarpine [3], and 14-acetyldictyocarpine [5] have been revised on the basis of a study of their 1D, 2D, and selective INEPT nmr spectra. These revisions suggest that the 13C-nmr chemical shift assignments for twenty-eight other norditerpenoid alkaloids possessing 7,8-methylenedioxy and 10 beta-OH groups may have to be revised. Complete 1H-nmr chemical shift assignments for compounds 1-3 and 5 are also reported |
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ISSN: | 0163-3864 1520-6025 |
DOI: | 10.1021/np50097a019 |