Selective 2H, 2H 1D-TOCSY NMR spectroscopy for signal assignment in perdeuteriated compounds

The 1D‐TOCSY experiment for 2H NMR is introduced and applications for signal assignments are illustrated with the spectra of pyridine‐d5 and iodo‐ and chlorocyclohexane‐d11. The potential of the method for the analysis of overlapping 2H spectra is demonstrated.

Gespeichert in:

Bibliographische Detailangaben
Veröffentlicht in:	Magnetic resonance in chemistry 1993-05, Vol.31 (5), p.509-511
Hauptverfasser:	Mons, Hans-Egbert, Bergander, Klaus, Günther, Harald
Format:	Artikel
Sprache:	eng
Schlagworte:	1D-TOCSY 2H NMR 2H-TOCSY Atomic and molecular physics Deuteriated cyclohexanes Exact sciences and technology Magnetization transfer Selective excitation Molecular properties and interactions with photons NMR Nuclear resonance and relaxation Physics Pyridine-d5
Online-Zugang:	Volltext
Tags:	Tag hinzufügen Keine Tags, Fügen Sie den ersten Tag hinzu!

Beschreibung
Zusammenfassung:	The 1D‐TOCSY experiment for 2H NMR is introduced and applications for signal assignments are illustrated with the spectra of pyridine‐d5 and iodo‐ and chlorocyclohexane‐d11. The potential of the method for the analysis of overlapping 2H spectra is demonstrated.
ISSN:	0749-1581 1097-458X
DOI:	10.1002/mrc.1260310517