Complete 1H and 13C NMR spectral assignment of some polynitropolycyclic cage molecules by 2D NMR spectroscopy

The 1H and 13C NMR spectra of several saturated polynitropolycyclic molecules were unambiguously assigned using aromatic solvent‐induced shifts, NOE difference spectra, 1H–1H COSY spectra and 2D 13C–1H shift correlated spectra, optimized either for one‐bond or long‐range 13C–1H couplings....

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Veröffentlicht in:	Magnetic resonance in chemistry 1991-01, Vol.29 (1), p.9-17
Hauptverfasser:	Axenrod, T., Liang, B., Dave, P. R.
Format:	Artikel
Sprache:	eng
Schlagworte:	2D long-range 13C-1H shift correlated spectra Aromatic solvent-induced shifts Atomic and molecular physics Exact sciences and technology Molecular properties and interactions with photons Nitro-substituted adamantanes Nitro-substituted pentacycloundecanes NOE difference spectra Nuclear resonance and relaxation Physics Polynitropolycyclic molecules
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Zusammenfassung:	The 1H and 13C NMR spectra of several saturated polynitropolycyclic molecules were unambiguously assigned using aromatic solvent‐induced shifts, NOE difference spectra, 1H–1H COSY spectra and 2D 13C–1H shift correlated spectra, optimized either for one‐bond or long‐range 13C–1H couplings.
ISSN:	0749-1581 1097-458X
DOI:	10.1002/mrc.1260290104