A versatile sample-environment cell for non-ambient X-ray scattering experiments

A versatile sample-environment cell for non-ambient X-ray scattering experiments

A compact reaction cell is described for in‐situ experiments requiring control of both the temperature of the sample and the atmosphere over the sample. The cell incorporates an optional furnace capable of temperatures of up to ∼1273 K. The compact design and ability of the cell to mount directly on...

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Veröffentlicht in:Journal of applied crystallography 2008-08, Vol.41 (4), p.822-824
Hauptverfasser: Chupas, Peter J., Chapman, Karena W., Kurtz, Charles, Hanson, Jonathan C., Lee, Peter L., Grey, Clare P.
Format: Artikel
Sprache:eng
Schlagworte:
Crystallography
DESIGN
DIFFRACTION
Experiments
flow-cells
FURNACES
GONIOMETERS
in-situ diffraction
non-ambient conditions
PARTICLE ACCELERATORS
Research methodology
SCATTERING
SYNCHROTRONS
Temperature
X-ray scattering
X-rays
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Beschreibung
Zusammenfassung:A compact reaction cell is described for in‐situ experiments requiring control of both the temperature of the sample and the atmosphere over the sample. The cell incorporates an optional furnace capable of temperatures of up to ∼1273 K. The compact design and ability of the cell to mount directly on a standard goniometer head allows portability to a large number of diffraction instruments at synchrotron sources.
ISSN:1600-5767
0021-8898
1600-5767
DOI:10.1107/S0021889808020165