Design and implementation of a simple and inexpensive GISAXS sample chamber

An in situ sample chamber designed for synchrotron grazing‐incidence small‐angle X‐ray scattering measurements of polymer film microstructure as a function of temperature is described. The chamber operates in a He environment and can be used to perform thermal quenching measurements for time‐depende...

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Veröffentlicht in:	Journal of applied crystallography 2006-02, Vol.39 (1), p.120-123
Hauptverfasser:	Groves, Michael N., Singh, Marsha A., Beydaghyan, Gisia, Muller, Matthew S., Sheridan, Emily, Schneider, Dieter K.
Format:	Artikel
Sprache:	eng
Schlagworte:	Condensed matter: structure, mechanical and thermal properties Crystalline state (including molecular motions in solids) Crystallographic aspects of phase transformations pressure effects DESIGN Exact sciences and technology grazing-incidence small-angle X-ray scattering (GISAXS) IMPLEMENTATION KINETICS MICROSTRUCTURE MONITORING national synchrotron light source NSLS PARTICLE ACCELERATORS PHASE TRANSFORMATIONS Physics polymer microstructure POLYMERS QUENCHING sample chambers SCATTERING Structure of solids and liquids crystallography synchrotron applications SYNCHROTRONS X-ray diffraction and scattering X-ray scattering (including small-angle scattering)
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Zusammenfassung:	An in situ sample chamber designed for synchrotron grazing‐incidence small‐angle X‐ray scattering measurements of polymer film microstructure as a function of temperature is described. The chamber operates in a He environment and can be used to perform thermal quenching measurements for time‐dependent monitoring of phase transformation kinetics. Preliminary data on a symmetric styrene–butadiene polymer are presented.
ISSN:	1600-5767 0021-8898 1600-5767
DOI:	10.1107/S0021889805041051