Synthesis and X-ray structures of metallocenium diamines of ironand cobalt

A detailed, reproducible synthesis of 1,10-diaminocobaltocenium hexafluorophosphate is provided. The compound can be made on gram scales in several steps starting from 1,10-dimethylcobaltoceniumsalts. The X-ray structures of 1,10-diamino cobaltoceniumhexafluorophosphate and a related 1,10-diamino fe...

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Veröffentlicht in:Polyhedron 2004-05, Vol.23
Hauptverfasser: Inyushin, Sviatoslav, Shafir, Alexandr, Sheats, John E., Minihane, Michael, Whitten Jr., Charles E., Arnold, John
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Sprache:eng
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Zusammenfassung:A detailed, reproducible synthesis of 1,10-diaminocobaltocenium hexafluorophosphate is provided. The compound can be made on gram scales in several steps starting from 1,10-dimethylcobaltoceniumsalts. The X-ray structures of 1,10-diamino cobaltoceniumhexafluorophosphate and a related 1,10-diamino ferrocenium salt, are described.
ISSN:0277-5387
DOI:10.1016/j.poly.2004.08.012