Mechanical properties of Al/ω-Al-Cu-Fe composites synthesized by the SPS technique

Al/40 vol%ω-Al-Cu-Fe composites were produced from Al powder and i-Al-Cu-Fe quasi-crystalline particles using spark plasma sintering (SPS) technique. The mechanical properties of the composite were evaluated over the temperature range 293 K–823 K by performing compression tests at constant strain ra...

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Veröffentlicht in:Materials characterization 2018-11, Vol.145, p.644-652
Hauptverfasser: Joseph, Aurélie, Gauthier-Brunet, Véronique, Joulain, Anne, Bonneville, Joël, Dubois, Sylvain, Monchoux, Jean-Philippe, Pailloux, Frédéric
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Sprache:eng
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Zusammenfassung:Al/40 vol%ω-Al-Cu-Fe composites were produced from Al powder and i-Al-Cu-Fe quasi-crystalline particles using spark plasma sintering (SPS) technique. The mechanical properties of the composite were evaluated over the temperature range 293 K–823 K by performing compression tests at constant strain rate. The temperature dependence of the σ0,2% yield stress gives evidence of two temperature regimes with a transition in the range 473 K–523 K. The decrease of σ0,2% with increasing temperature, more pronounced in the low temperature regime, indicates that the two temperature regimes correspond to two different thermally activated deformation mechanisms. Based on microstructural analyses of the Al matrix, where plastic deformation takes place, the different strengthening contributions are discussed and the results are finally compared to those obtained for composites produced by hot isostatic pressing (HIP), for which the σ0,2% temperature dependence is similar. In the low temperature regime, the σ0.2% stress of the SPS composites is higher than that of the HIP composites. In this temperature regime, the stress difference is mainly ascribed to the different reinforcement phases present in the Al matrix. In the high temperature regime, the temperature dependence of σ0.2% is comparable for the two composites whatever the processing route: load transfer is thus the main strengthening mechanism, which is similar for the two Al/ω-Al-Cu-Fe composites, the temperature dependence being ascribed to cross slip and climb processes. •For the first time, Al/ω-Al-Cu-Fe composites are produced by Spark Plasma Sintering.•Cu diffusion in Al matrix leads to precipitation of θ′-Al2Cu.•The σ0.2% drop at around 523 K is due to coarsening of θ′-Al2Cu precipitates.•At high temperature, load transfer is the main strengthening mechanism.•At low temperature, SPS Al/ω composites have higher σ0.2% than HIP Al/ω composites.
ISSN:1044-5803
1873-4189
DOI:10.1016/j.matchar.2018.09.025