Hydrothermal synthesis and infrared emissivity property of flower-like SnO{sub 2} particles
The flower-like SnO{sub 2} particles are synthesized through a simple hydrothermal process. The microstructure, morphology and the infrared emissivity property of the as-prepared products are characterized by x-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microsco...
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Veröffentlicht in: | AIP advances 2014-04, Vol.4 (4) |
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Hauptverfasser: | , , , , , , , , |
Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | The flower-like SnO{sub 2} particles are synthesized through a simple hydrothermal process. The microstructure, morphology and the infrared emissivity property of the as-prepared products are characterized by x-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscope (TEM), and infrared spectroradio meter (ISM) respectively. The results show that the as-prepared SnO{sub 2} products are all indexed to tetragonal cassiterite phase of SnO{sub 2}. The different molarity ratios of the OH{sup −} concentration to Sn{sup 4+} concentration ([OH{sup −}]:[Sn{sup 4+}]) and the polyacrylamide (PAM) lead to the different morphological structures of SnO{sub 2}, which indicates that both the [OH{sup −}]:[Sn{sup 4+}] and the PAM play an important role in the morphological evolution respectively. The infrared emissivities of the as-prepared SnO{sub 2} products are discussed. |
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ISSN: | 2158-3226 2158-3226 |
DOI: | 10.1063/1.4873536 |