Hydrothermal synthesis and infrared emissivity property of flower-like SnO{sub 2} particles

The flower-like SnO{sub 2} particles are synthesized through a simple hydrothermal process. The microstructure, morphology and the infrared emissivity property of the as-prepared products are characterized by x-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microsco...

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Veröffentlicht in:AIP advances 2014-04, Vol.4 (4)
Hauptverfasser: Tian, J. X., Beijing Institute of Environmental Features, Beijing, 100854, Zhang, Z. Y., School of Information Science and Technology, Northwest University, Xi'an 710127, Yan, J. F., Ruan, X. F., Yun, J. N., Zhao, W., Zhai, C. X.
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Sprache:eng
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Zusammenfassung:The flower-like SnO{sub 2} particles are synthesized through a simple hydrothermal process. The microstructure, morphology and the infrared emissivity property of the as-prepared products are characterized by x-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscope (TEM), and infrared spectroradio meter (ISM) respectively. The results show that the as-prepared SnO{sub 2} products are all indexed to tetragonal cassiterite phase of SnO{sub 2}. The different molarity ratios of the OH{sup −} concentration to Sn{sup 4+} concentration ([OH{sup −}]:[Sn{sup 4+}]) and the polyacrylamide (PAM) lead to the different morphological structures of SnO{sub 2}, which indicates that both the [OH{sup −}]:[Sn{sup 4+}] and the PAM play an important role in the morphological evolution respectively. The infrared emissivities of the as-prepared SnO{sub 2} products are discussed.
ISSN:2158-3226
2158-3226
DOI:10.1063/1.4873536