Synthesis and microstructural control of flower-like cadmium germanate

Flower-like Cd 2Ge 2O 6 have been synthesized using a facile hydrothermal process with ethylenediamine. The roles of hydrothermal conditions on the size and morphology of the flower-like Cd 2Ge 2O 6 were investigated. The research results show that the obtained Cd 2Ge 2O 6 presents a flower-like mic...

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Veröffentlicht in:Materials characterization 2011-11, Vol.62 (11), p.1029-1035
Hauptverfasser: Pei, L.Z., Yang, Y., Pei, Y.Q., Ran, S.L.
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Sprache:eng
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Zusammenfassung:Flower-like Cd 2Ge 2O 6 have been synthesized using a facile hydrothermal process with ethylenediamine. The roles of hydrothermal conditions on the size and morphology of the flower-like Cd 2Ge 2O 6 were investigated. The research results show that the obtained Cd 2Ge 2O 6 presents a flower-like microstructures composed by radial nanorods with diameter of 50–100 nm and length of 0.5–2 μm, respectively. The formation mechanism of the flower-like Cd 2Ge 2O 6 is explained according to the ethylenediamine-assisted nucleation-“Ostwald ripening” process. ►Cd 2Ge 2O 6 flower-like microstructures were synthesized using ethylenediamine. ►Cd 2Ge 2O 6 flower-like microstructures can be controlled by growth conditions. ►Ethylenediamine induces the growth of the Cd 2Ge 2O 6 flower-like microstructures.
ISSN:1044-5803
1873-4189
DOI:10.1016/j.matchar.2011.08.001