Synthesis and microstructural control of flower-like cadmium germanate
Flower-like Cd 2Ge 2O 6 have been synthesized using a facile hydrothermal process with ethylenediamine. The roles of hydrothermal conditions on the size and morphology of the flower-like Cd 2Ge 2O 6 were investigated. The research results show that the obtained Cd 2Ge 2O 6 presents a flower-like mic...
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Veröffentlicht in: | Materials characterization 2011-11, Vol.62 (11), p.1029-1035 |
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Hauptverfasser: | , , , |
Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | Flower-like Cd
2Ge
2O
6 have been synthesized using a facile hydrothermal process with ethylenediamine. The roles of hydrothermal conditions on the size and morphology of the flower-like Cd
2Ge
2O
6 were investigated. The research results show that the obtained Cd
2Ge
2O
6 presents a flower-like microstructures composed by radial nanorods with diameter of 50–100
nm and length of 0.5–2
μm, respectively. The formation mechanism of the flower-like Cd
2Ge
2O
6 is explained according to the ethylenediamine-assisted nucleation-“Ostwald ripening” process.
►Cd
2Ge
2O
6 flower-like microstructures were synthesized using ethylenediamine. ►Cd
2Ge
2O
6 flower-like microstructures can be controlled by growth conditions. ►Ethylenediamine induces the growth of the Cd
2Ge
2O
6 flower-like microstructures. |
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ISSN: | 1044-5803 1873-4189 |
DOI: | 10.1016/j.matchar.2011.08.001 |