Synchrotron x-ray powder diffraction studies in pulsed magnetic fields
X-ray powder diffraction experiments under pulsed magnetic fields were carried out at the DUBBLE beamline (BM26B) at the ESRF. A mobile generator delivered 110 kJ to the magnet coil, which was sufficient to generate peak fields of 30 T . A liquid He flow cryostat allowed us to vary the sample temper...
Gespeichert in:
Veröffentlicht in: | Review of scientific instruments 2006-06, Vol.77 (6), p.063903-063903-8 |
---|---|
Hauptverfasser: | , , , , , , , , , |
Format: | Artikel |
Sprache: | eng |
Schlagworte: | |
Online-Zugang: | Volltext |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
Zusammenfassung: | X-ray powder diffraction experiments under pulsed magnetic fields were carried out at the DUBBLE beamline (BM26B) at the ESRF. A mobile generator delivered
110
kJ
to the magnet coil, which was sufficient to generate peak fields of
30
T
. A liquid He flow cryostat allowed us to vary the sample temperature accurately between 8 and
300
K
. Powder diffraction patterns of several samples were recorded using
21
keV
monochromatic x-rays and an on-line image plate detector. Here we present the first results on the suppression of the Jahn-Teller structural distortion in
Tb
V
O
4
by magnetic field. These data clearly demonstrate the feasibility of x-ray powder diffraction experiments under pulsed magnetic fields with relatively inexpensive instrumentation. |
---|---|
ISSN: | 0034-6748 1089-7623 |
DOI: | 10.1063/1.2216914 |