Synchrotron x-ray powder diffraction studies in pulsed magnetic fields

X-ray powder diffraction experiments under pulsed magnetic fields were carried out at the DUBBLE beamline (BM26B) at the ESRF. A mobile generator delivered 110 kJ to the magnet coil, which was sufficient to generate peak fields of 30 T . A liquid He flow cryostat allowed us to vary the sample temper...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Review of scientific instruments 2006-06, Vol.77 (6), p.063903-063903-8
Hauptverfasser: Frings, P., Vanacken, J., Detlefs, C., Duc, F., Lorenzo, J. E., Nardone, M., Billette, J., Zitouni, A., Bras, W., Rikken, G. L. J. A.
Format: Artikel
Sprache:eng
Schlagworte:
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:X-ray powder diffraction experiments under pulsed magnetic fields were carried out at the DUBBLE beamline (BM26B) at the ESRF. A mobile generator delivered 110 kJ to the magnet coil, which was sufficient to generate peak fields of 30 T . A liquid He flow cryostat allowed us to vary the sample temperature accurately between 8 and 300 K . Powder diffraction patterns of several samples were recorded using 21 keV monochromatic x-rays and an on-line image plate detector. Here we present the first results on the suppression of the Jahn-Teller structural distortion in Tb V O 4 by magnetic field. These data clearly demonstrate the feasibility of x-ray powder diffraction experiments under pulsed magnetic fields with relatively inexpensive instrumentation.
ISSN:0034-6748
1089-7623
DOI:10.1063/1.2216914