One-step synthesis of electrically conductive polyaniline nanostructures by oxidative polymerization method

A simple, rapid and efficient route to prepare polyaniline nanostructures (PANI-NS) by “one-step chemical oxidative polymerization” method is described. This method possesses advantages in terms of good yield, short reaction time, neat conditions and cost-effectiveness. The morphology of the PANI-NS...

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Veröffentlicht in:Journal of industrial and engineering chemistry (Seoul, Korea) 2012, 18(4), , pp.1213-1215
Hauptverfasser: Ragupathy, Dhanusuraman, Gomathi, Palanisamy, Lee, Soo Chool, Al-Deyab, Salem S., Lee, Sang Hak, Ghim, Han Do
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Sprache:eng
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Zusammenfassung:A simple, rapid and efficient route to prepare polyaniline nanostructures (PANI-NS) by “one-step chemical oxidative polymerization” method is described. This method possesses advantages in terms of good yield, short reaction time, neat conditions and cost-effectiveness. The morphology of the PANI-NS was investigated by field-emission scanning electron microscopy (FE-SEM). The average diameter of single PANI-NS was calculated to be ∼376nm. Results from UV–visible spectroscopy, Fourier transform infrared spectroscopy, thermogravimetric analysis and cyclic voltammetry (CV) reveals the existence of PANI units present in the polymeric nanostructures. Also, electrical conducting property of the PANI-NS was analyzed using four-probe measurement method.
ISSN:1226-086X
1876-794X
DOI:10.1016/j.jiec.2012.01.032