NaHSO4/SiO2: An Efficient Catalyst for the Synthesis of β-Enaminones and 2-Methylquinolin-4(1H)-Ones under Solvent-Free Condition

An efficient and simplified protocol for NaHSO4/SiO2 catalyzed solvent-free synthesis of β-enaminone and 2-methylquinolin-4(1H)-one derivatives under microwave irradiation is described. A series of functionalized derivatives have been synthesized in shorter reaction times with moderate to good yield...

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Veröffentlicht in:Journal of the Korean Chemical Society 2010, 54(6), , pp.723-726
Hauptverfasser: Sapkal, Suryakant B, Shelke, Kiran F, Shingate, Bapurao B, Shingare, Murlidhar S
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Sprache:eng
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Zusammenfassung:An efficient and simplified protocol for NaHSO4/SiO2 catalyzed solvent-free synthesis of β-enaminone and 2-methylquinolin-4(1H)-one derivatives under microwave irradiation is described. A series of functionalized derivatives have been synthesized in shorter reaction times with moderate to good yields. The use of milder catalyst in non-conventional method offers significant advantages over conventional methods, such as higher selectivities, simplicity, solvent-free reaction and non-environmental polluting conditions. KCI Citation Count: 0
ISSN:1017-2548
2234-8530
DOI:10.5012/jkcs.2010.54.6.723