Indium Modified Mesoporous Zeolite AlMCM-41 as a Heterogeneous Catalyst for the Knoevenagel Condensation Reaction

The Indium modified mesoporous zeolite AlMCM-41 were synthesized by hydrothermal method and characterized by powder X-ray diffraction (XRD), fourier transform infrared spectroscopy (FT-IR) and scanning electron microscopy with energy dispersive spectroscopy (SEM-EDS) techniques. The Knoevenagel cond...

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Veröffentlicht in:Bulletin of the Korean Chemical Society 2010, 31(5), , pp.1301-1304
Hauptverfasser: Santosh S. Katkar, Machhindra K. Lande, Balasaheb R. Arbad, Sandip B. Rathod
Format: Artikel
Sprache:eng
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Zusammenfassung:The Indium modified mesoporous zeolite AlMCM-41 were synthesized by hydrothermal method and characterized by powder X-ray diffraction (XRD), fourier transform infrared spectroscopy (FT-IR) and scanning electron microscopy with energy dispersive spectroscopy (SEM-EDS) techniques. The Knoevenagel condensation of aldehyde with malononitrile or ethyl cyanoacetate was carried out at reflux condition in ethanol by using heterogeneous In/AlMCM-41catalyst. This method is fast, efficient, easy work-up and eco-friendly to afford the corresponding Knoevenagel adducts. The catalyst was recovered and reused for several cycles with consistent activity. KCI Citation Count: 12
ISSN:0253-2964
1229-5949
DOI:10.5012/bkcs.2010.31.5.1301