Elimination of the baseline distortions in WURST-CPMG static experiments
The WURST-CPMG pulse sequence enables: (i) observing very broad spectra due to WURST excitation, and (ii) increasing the S/N ratio due to CPMG acquisition. However, strong baseline distortions may be observed, which make the extraction of the tensor information difficult. We propose a slight modific...
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Veröffentlicht in: | Solid state nuclear magnetic resonance 2016-09, Vol.78, p.1-4 |
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Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | The WURST-CPMG pulse sequence enables: (i) observing very broad spectra due to WURST excitation, and (ii) increasing the S/N ratio due to CPMG acquisition. However, strong baseline distortions may be observed, which make the extraction of the tensor information difficult. We propose a slight modification of the sequence, WURST-CPMGM, in which we skip the first M echoes and we only acquire the following ones. This simple treatment mostly eliminates the strong background signal and the ring down effects, leading to a flat baseline.
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•WURST-CPMGM: skip the first M echoes and only acquire the following ones.•WURST-CPMGM could eliminate the strong background signal. |
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ISSN: | 0926-2040 1527-3326 |
DOI: | 10.1016/j.ssnmr.2016.05.002 |