One-pot synthesis of novel poly-substituted phenanthrenes

One-pot synthesis of novel poly-substituted phenanthrenes

A one-pot synthesis of novel poly-substituted phenanthrenes is described in this article through a Suzuki–Miyaura cross-coupling followed by a Dieckmann–Thorpe ring closure under microwave irradiation. The selection of the appropriate starting materials allowed us to introduce diversity on various p...

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Veröffentlicht in:Tetrahedron 2010-04, Vol.66 (15), p.2803-2808
Hauptverfasser: Yougnia, Rodrigue, Rochais, Christophe, Oliveira Santos, Jana Sopkovà-de, Dallemagne, Patrick, Rault, Sylvain
Format: Artikel
Sprache:eng
Schlagworte:
Chemical Sciences
Chemistry
Condensed benzenic and aromatic compounds
Dieckmann–Thorpe
Exact sciences and technology
Fused ring system
Organic chemistry
Phenanthrene
Preparations and properties
Ring closure
Suzuki–Miyaura cross-coupling
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Zusammenfassung:A one-pot synthesis of novel poly-substituted phenanthrenes is described in this article through a Suzuki–Miyaura cross-coupling followed by a Dieckmann–Thorpe ring closure under microwave irradiation. The selection of the appropriate starting materials allowed us to introduce diversity on various positions of the phenanthrene ring system. [Display omitted]
ISSN:0040-4020
1464-5416
DOI:10.1016/j.tet.2010.02.060