Synthesis and Structure of New Macrocycles Including Spiro-1,3-Dioxane Units

Synthesis and Structure of New Macrocycles Including Spiro-1,3-Dioxane Units

The efficient synthesis of new macrocycles — “monomers” and “dimers” — containing spiro‐1,3‐dioxane units is reported. The structure of the compounds was determined from high‐field NMR spectra, FAB and MALDI+ mass spectrometry investigations. The solid‐state molecular structures of three compounds w...

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Veröffentlicht in:European journal of organic chemistry 2003-08, Vol.2003 (16), p.3153-3161
Hauptverfasser: Grosu, Ion, Bogdan, Elena, Plé, Gérard, Toupet, Loïc, Ramondenc, Yvan, Condamine, Eric, Peulon-Agasse, Valérie, Balog, Mirela
Format: Artikel
Sprache:eng
Schlagworte:
Analytical chemistry
Chemical Sciences
Host-guest systems
Macrocycles
Material chemistry
Organic chemistry
Oxygen heterocycles
Spiro compounds
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Zusammenfassung:The efficient synthesis of new macrocycles — “monomers” and “dimers” — containing spiro‐1,3‐dioxane units is reported. The structure of the compounds was determined from high‐field NMR spectra, FAB and MALDI+ mass spectrometry investigations. The solid‐state molecular structures of three compounds was determined. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2003)
ISSN:1434-193X
1099-0690
DOI:10.1002/ejoc.200200615